      Table 1.  Crystal data and structure refinement for bas07. 
  
  
      Identification code               bas07 
  
      Empirical formula                 C38 H54 Cl2 Cr N3 O2 
  
      Formula weight                    707.74 
  
      Temperature                       223(2) K 
  
      Wavelength                        0.71073 A 
  
      Crystal system, space group       Triclinic,  P-1 
  
      Unit cell dimensions              a = 11.164(12) A   alpha = 108.56(2) deg. 
                                        b = 11.976(13) A    beta = 104.16(2) deg. 
                                        c = 15.387(16) A   gamma = 93.04(2) deg. 
  
      Volume                            1872(3) A^3 
  
      Z, Calculated density             2,  1.256 Mg/m^3 
  
      Absorption coefficient            0.484 mm^-1 
  
      F(000)                            754 
  
      Crystal size                      0.25 x 0.25 x 0.15 mm 
  
      Theta range for data collection   1.45 to 28.42 deg. 
  
      Limiting indices                  -14<=h<=13, -10<=k<=15, -19<=l<=18 
  
      Reflections collected / unique    10040 / 6959 [R(int) = 0.0369] 
  
      Completeness to theta = 22.50     85.5 % 
  
      Absorption correction             Semi-empirical from equivalents 
  
      Max. and min. transmission        0.9309 and 0.8886 
  
      Refinement method                 Full-matrix least-squares on F^2 
  
      Data / restraints / parameters    6959 / 0 / 423 
  
      Goodness-of-fit on F^2            1.016 
  
      Final R indices [I>2sigma(I)]     R1 = 0.0591, wR2 = 0.1463 
  
      R indices (all data)              R1 = 0.0945, wR2 = 0.1658 
  
      Largest diff. peak and hole       0.540 and -0.299 e.A^-3 
  
         Table 2.  Atomic coordinates ( x 10^4) and equivalent isotropic 
         displacement parameters (A^2 x 10^3) for bas07. 
         U(eq) is defined as one third of the trace of the orthogonalized 
         Uij tensor. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          Cr(1)        7887(1)       3372(1)       1111(1)       32(1) 
          Cl(1)        9154(1)       4999(1)       2262(1)       48(1) 
          Cl(2)        7410(1)       4305(1)         -2(1)       50(1) 
          O(1)         6344(2)       3897(2)       1505(2)       40(1) 
          O(2)         9379(2)       2814(2)        621(2)       39(1) 
          N(1)         8214(2)       2473(3)       2111(2)       30(1) 
          N(2)         6907(2)       1723(3)        243(2)       29(1) 
          N(3)         5230(2)        922(3)      -2264(2)       37(1) 
          C(1)         8842(3)       2872(3)       3135(2)       33(1) 
          C(2)         8139(3)       3176(3)       3787(2)       40(1) 
          C(3)         8758(4)       3469(4)       4758(3)       51(1) 
          C(4)        10015(4)       3458(4)       5064(3)       60(1) 
          C(5)        10689(4)       3182(4)       4410(3)       55(1) 
          C(6)        10134(3)       2885(4)       3430(2)       44(1) 
          C(7)        10908(3)       2560(5)       2736(3)       57(1) 
          C(8)        11282(5)       1327(5)       2614(4)       84(2) 
          C(9)        12059(4)       3479(6)       3030(4)       87(2) 
          C(10)        6729(3)       3179(4)       3489(3)       45(1) 
          C(11)        6330(4)       4271(4)       4129(3)       68(1) 
          C(12)        6009(4)       2070(4)       3453(3)       59(1) 
          C(13)        7763(3)       1370(3)       1709(2)       32(1) 
          C(14)        7098(3)        916(3)        718(2)       30(1) 
          C(15)        6616(3)       -227(3)        102(2)       35(1) 
          C(16)        6105(3)       -140(3)       -793(2)       37(1) 
          C(17)        6285(3)       1051(3)       -688(2)       31(1) 
          C(18)        5858(3)       1575(3)      -1425(2)       33(1) 
          C(19)        4868(3)       1463(3)      -2972(2)       33(1) 
          C(20)        3587(3)       1491(3)      -3327(2)       39(1) 
          C(21)        3209(3)       1990(4)      -4030(3)       50(1) 
          C(22)        4067(4)       2429(4)      -4384(3)       52(1) 
          C(23)        5307(3)       2347(4)      -4062(3)       48(1) 
          C(24)        5741(3)       1868(3)      -3347(2)       39(1) 
          C(25)        2651(3)        988(4)      -2943(3)       47(1) 
          C(26)        2378(5)       1913(5)      -2116(4)       80(2) 
          C(27)        1445(4)        331(5)      -3709(4)       84(2) 
          C(28)        7121(3)       1742(5)      -3059(3)       58(1) 
          C(29)        7939(4)       2928(6)      -2634(4)       97(2) 
          C(30)        7502(5)        958(6)      -3911(4)       99(2) 
          C(31)        5117(3)       3318(4)        931(3)       59(1) 
          C(32)        4280(4)       3985(5)       1476(4)       78(2) 
          C(33)        4924(5)       5216(5)       1919(4)      106(3) 
          C(34)        6260(4)       5146(4)       1984(3)       65(1) 
          C(35)       10324(4)       3651(4)        545(3)       55(1) 
          C(36)       10766(5)       2965(5)       -263(4)       85(2) 
          C(37)       10546(6)       1730(6)       -316(6)      110(2) 
          C(38)        9469(4)       1644(4)         35(4)       65(1) 
         ________________________________________________________________ 
  
           Table 3.  Bond lengths [A] and angles [deg] for bas07. 
           _____________________________________________________________ 
  
            Cr(1)-O(1)                    2.028(3) 
            Cr(1)-O(2)                    2.050(3) 
            Cr(1)-N(2)                    2.064(3) 
            Cr(1)-N(1)                    2.116(3) 
            Cr(1)-Cl(1)                   2.284(2) 
            Cr(1)-Cl(2)                   2.302(2) 
            O(1)-C(31)                    1.434(4) 
            O(1)-C(34)                    1.462(5) 
            O(2)-C(38)                    1.429(5) 
            O(2)-C(35)                    1.468(4) 
            N(1)-C(13)                    1.280(4) 
            N(1)-C(1)                     1.465(4) 
            N(2)-C(17)                    1.379(4) 
            N(2)-C(14)                    1.381(4) 
            N(3)-C(18)                    1.275(4) 
            N(3)-C(19)                    1.426(4) 
            C(1)-C(2)                     1.392(5) 
            C(1)-C(6)                     1.401(5) 
            C(2)-C(3)                     1.403(5) 
            C(2)-C(10)                    1.529(5) 
            C(3)-C(4)                     1.369(6) 
            C(3)-H(3A)                    0.9400 
            C(4)-C(5)                     1.369(6) 
            C(4)-H(4A)                    0.9400 
            C(5)-C(6)                     1.400(5) 
            C(5)-H(5A)                    0.9400 
            C(6)-C(7)                     1.504(6) 
            C(7)-C(8)                     1.522(7) 
            C(7)-C(9)                     1.521(6) 
            C(7)-H(7A)                    0.9900 
            C(8)-H(8A)                    0.9700 
            C(8)-H(8B)                    0.9700 
            C(8)-H(8C)                    0.9700 
            C(9)-H(9A)                    0.9700 
            C(9)-H(9B)                    0.9700 
            C(9)-H(9C)                    0.9700 
            C(10)-C(12)                   1.493(6) 
            C(10)-C(11)                   1.528(6) 
            C(10)-H(10A)                  0.9900 
            C(11)-H(11A)                  0.9700 
            C(11)-H(11B)                  0.9700 
            C(11)-H(11C)                  0.9700 
            C(12)-H(12A)                  0.9700 
            C(12)-H(12B)                  0.9700 
            C(12)-H(12C)                  0.9700 
            C(13)-C(14)                   1.430(4) 
            C(13)-H(13A)                  0.9400 
            C(14)-C(15)                   1.382(5) 
            C(15)-C(16)                   1.395(4) 
            C(15)-H(15A)                  0.9400 
            C(16)-C(17)                   1.381(5) 
            C(16)-H(16A)                  0.9400 
            C(17)-C(18)                   1.459(4) 
            C(18)-H(18A)                  0.9400 
            C(19)-C(24)                   1.386(5) 
            C(19)-C(20)                   1.408(5) 
            C(20)-C(21)                   1.386(5) 
            C(20)-C(25)                   1.504(5) 
            C(21)-C(22)                   1.369(6) 
            C(21)-H(21A)                  0.9400 
            C(22)-C(23)                   1.372(5) 
            C(22)-H(22A)                  0.9400 
            C(23)-C(24)                   1.394(5) 
            C(23)-H(23A)                  0.9400 
            C(24)-C(28)                   1.524(5) 
            C(25)-C(26)                   1.506(6) 
            C(25)-C(27)                   1.531(5) 
            C(25)-H(25A)                  0.9900 
            C(26)-H(26A)                  0.9700 
            C(26)-H(26B)                  0.9700 
            C(26)-H(26C)                  0.9700 
            C(27)-H(27A)                  0.9700 
            C(27)-H(27B)                  0.9700 
            C(27)-H(27C)                  0.9700 
            C(28)-C(29)                   1.503(7) 
            C(28)-C(30)                   1.521(7) 
            C(28)-H(28A)                  0.9900 
            C(29)-H(29A)                  0.9700 
            C(29)-H(29B)                  0.9700 
            C(29)-H(29C)                  0.9700 
            C(30)-H(30A)                  0.9700 
            C(30)-H(30B)                  0.9700 
            C(30)-H(30C)                  0.9700 
            C(31)-C(32)                   1.501(6) 
            C(31)-H(31A)                  0.9800 
            C(31)-H(31B)                  0.9800 
            C(32)-C(33)                   1.471(7) 
            C(32)-H(32A)                  0.9800 
            C(32)-H(32B)                  0.9800 
            C(33)-C(34)                   1.479(7) 
            C(33)-H(33A)                  0.9800 
            C(33)-H(33B)                  0.9800 
            C(34)-H(34A)                  0.9800 
            C(34)-H(34B)                  0.9800 
            C(35)-C(36)                   1.468(7) 
            C(35)-H(35A)                  0.9800 
            C(35)-H(35B)                  0.9800 
            C(36)-C(37)                   1.460(8) 
            C(36)-H(36A)                  0.9800 
            C(36)-H(36B)                  0.9800 
            C(37)-C(38)                   1.445(6) 
            C(37)-H(37A)                  0.9800 
            C(37)-H(37B)                  0.9800 
            C(38)-H(38A)                  0.9800 
            C(38)-H(38B)                  0.9800 
  
            O(1)-Cr(1)-O(2)             176.20(9) 
            O(1)-Cr(1)-N(2)              90.87(12) 
            O(2)-Cr(1)-N(2)              86.94(12) 
            O(1)-Cr(1)-N(1)              89.87(11) 
            O(2)-Cr(1)-N(1)              92.86(11) 
            N(2)-Cr(1)-N(1)              80.93(13) 
            O(1)-Cr(1)-Cl(1)             92.50(10) 
            O(2)-Cr(1)-Cl(1)             90.24(10) 
            N(2)-Cr(1)-Cl(1)            168.66(8) 
            N(1)-Cr(1)-Cl(1)             88.25(11) 
            O(1)-Cr(1)-Cl(2)             87.71(9) 
            O(2)-Cr(1)-Cl(2)             89.46(9) 
            N(2)-Cr(1)-Cl(2)             96.78(11) 
            N(1)-Cr(1)-Cl(2)            176.64(7) 
            Cl(1)-Cr(1)-Cl(2)            94.17(9) 
            C(31)-O(1)-C(34)            107.9(3) 
            C(31)-O(1)-Cr(1)            121.3(3) 
            C(34)-O(1)-Cr(1)            122.1(2) 
            C(38)-O(2)-C(35)            108.0(3) 
            C(38)-O(2)-Cr(1)            127.1(2) 
            C(35)-O(2)-Cr(1)            121.8(3) 
            C(13)-N(1)-C(1)             116.6(3) 
            C(13)-N(1)-Cr(1)            110.8(2) 
            C(1)-N(1)-Cr(1)             132.6(2) 
            C(17)-N(2)-C(14)            105.2(3) 
            C(17)-N(2)-Cr(1)            143.5(2) 
            C(14)-N(2)-Cr(1)            110.1(2) 
            C(18)-N(3)-C(19)            118.6(3) 
            C(2)-C(1)-C(6)              121.6(3) 
            C(2)-C(1)-N(1)              119.6(3) 
            C(6)-C(1)-N(1)              118.8(3) 
            C(1)-C(2)-C(3)              118.1(3) 
            C(1)-C(2)-C(10)             122.9(3) 
            C(3)-C(2)-C(10)             119.0(3) 
            C(4)-C(3)-C(2)              121.5(4) 
            C(4)-C(3)-H(3A)             119.3 
            C(2)-C(3)-H(3A)             119.3 
            C(5)-C(4)-C(3)              119.3(3) 
            C(5)-C(4)-H(4A)             120.3 
            C(3)-C(4)-H(4A)             120.3 
            C(4)-C(5)-C(6)              122.3(4) 
            C(4)-C(5)-H(5A)             118.9 
            C(6)-C(5)-H(5A)             118.9 
            C(5)-C(6)-C(1)              117.2(4) 
            C(5)-C(6)-C(7)              120.4(3) 
            C(1)-C(6)-C(7)              122.3(3) 
            C(6)-C(7)-C(8)              111.4(4) 
            C(6)-C(7)-C(9)              111.7(4) 
            C(8)-C(7)-C(9)              110.3(4) 
            C(6)-C(7)-H(7A)             107.7 
            C(8)-C(7)-H(7A)             107.7 
            C(9)-C(7)-H(7A)             107.7 
            C(7)-C(8)-H(8A)             109.5 
            C(7)-C(8)-H(8B)             109.5 
            H(8A)-C(8)-H(8B)            109.5 
            C(7)-C(8)-H(8C)             109.5 
            H(8A)-C(8)-H(8C)            109.5 
            H(8B)-C(8)-H(8C)            109.5 
            C(7)-C(9)-H(9A)             109.5 
            C(7)-C(9)-H(9B)             109.5 
            H(9A)-C(9)-H(9B)            109.5 
            C(7)-C(9)-H(9C)             109.5 
            H(9A)-C(9)-H(9C)            109.5 
            H(9B)-C(9)-H(9C)            109.5 
            C(12)-C(10)-C(11)           110.1(4) 
            C(12)-C(10)-C(2)            112.4(3) 
            C(11)-C(10)-C(2)            112.2(3) 
            C(12)-C(10)-H(10A)          107.3 
            C(11)-C(10)-H(10A)          107.3 
            C(2)-C(10)-H(10A)           107.3 
            C(10)-C(11)-H(11A)          109.5 
            C(10)-C(11)-H(11B)          109.5 
            H(11A)-C(11)-H(11B)         109.5 
            C(10)-C(11)-H(11C)          109.5 
            H(11A)-C(11)-H(11C)         109.5 
            H(11B)-C(11)-H(11C)         109.5 
            C(10)-C(12)-H(12A)          109.5 
            C(10)-C(12)-H(12B)          109.5 
            H(12A)-C(12)-H(12B)         109.5 
            C(10)-C(12)-H(12C)          109.5 
            H(12A)-C(12)-H(12C)         109.5 
            H(12B)-C(12)-H(12C)         109.5 
            N(1)-C(13)-C(14)            120.2(3) 
            N(1)-C(13)-H(13A)           119.9 
            C(14)-C(13)-H(13A)          119.9 
            N(2)-C(14)-C(15)            110.7(3) 
            N(2)-C(14)-C(13)            117.4(3) 
            C(15)-C(14)-C(13)           131.9(3) 
            C(14)-C(15)-C(16)           106.5(3) 
            C(14)-C(15)-H(15A)          126.7 
            C(16)-C(15)-H(15A)          126.7 
            C(17)-C(16)-C(15)           107.0(3) 
            C(17)-C(16)-H(16A)          126.5 
            C(15)-C(16)-H(16A)          126.5 
            C(16)-C(17)-N(2)            110.5(3) 
            C(16)-C(17)-C(18)           126.6(3) 
            N(2)-C(17)-C(18)            122.9(3) 
            N(3)-C(18)-C(17)            120.4(3) 
            N(3)-C(18)-H(18A)           119.8 
            C(17)-C(18)-H(18A)          119.8 
            C(24)-C(19)-C(20)           121.2(3) 
            C(24)-C(19)-N(3)            121.0(3) 
            C(20)-C(19)-N(3)            117.7(3) 
            C(21)-C(20)-C(19)           118.8(3) 
            C(21)-C(20)-C(25)           121.0(3) 
            C(19)-C(20)-C(25)           120.2(3) 
            C(22)-C(21)-C(20)           120.5(3) 
            C(22)-C(21)-H(21A)          119.8 
            C(20)-C(21)-H(21A)          119.8 
            C(21)-C(22)-C(23)           120.1(4) 
            C(21)-C(22)-H(22A)          120.0 
            C(23)-C(22)-H(22A)          120.0 
            C(22)-C(23)-C(24)           121.9(4) 
            C(22)-C(23)-H(23A)          119.1 
            C(24)-C(23)-H(23A)          119.1 
            C(19)-C(24)-C(23)           117.5(3) 
            C(19)-C(24)-C(28)           123.1(3) 
            C(23)-C(24)-C(28)           119.2(3) 
            C(20)-C(25)-C(26)           112.3(4) 
            C(20)-C(25)-C(27)           113.4(3) 
            C(26)-C(25)-C(27)           111.1(4) 
            C(20)-C(25)-H(25A)          106.5 
            C(26)-C(25)-H(25A)          106.5 
            C(27)-C(25)-H(25A)          106.5 
            C(25)-C(26)-H(26A)          109.5 
            C(25)-C(26)-H(26B)          109.5 
            H(26A)-C(26)-H(26B)         109.5 
            C(25)-C(26)-H(26C)          109.5 
            H(26A)-C(26)-H(26C)         109.5 
            H(26B)-C(26)-H(26C)         109.5 
            C(25)-C(27)-H(27A)          109.5 
            C(25)-C(27)-H(27B)          109.5 
            H(27A)-C(27)-H(27B)         109.5 
            C(25)-C(27)-H(27C)          109.5 
            H(27A)-C(27)-H(27C)         109.5 
            H(27B)-C(27)-H(27C)         109.5 
            C(29)-C(28)-C(24)           112.0(4) 
            C(29)-C(28)-C(30)           109.9(4) 
            C(24)-C(28)-C(30)           110.5(4) 
            C(29)-C(28)-H(28A)          108.1 
            C(24)-C(28)-H(28A)          108.1 
            C(30)-C(28)-H(28A)          108.1 
            C(28)-C(29)-H(29A)          109.5 
            C(28)-C(29)-H(29B)          109.5 
            H(29A)-C(29)-H(29B)         109.5 
            C(28)-C(29)-H(29C)          109.5 
            H(29A)-C(29)-H(29C)         109.5 
            H(29B)-C(29)-H(29C)         109.5 
            C(28)-C(30)-H(30A)          109.5 
            C(28)-C(30)-H(30B)          109.5 
            H(30A)-C(30)-H(30B)         109.5 
            C(28)-C(30)-H(30C)          109.5 
            H(30A)-C(30)-H(30C)         109.5 
            H(30B)-C(30)-H(30C)         109.5 
            O(1)-C(31)-C(32)            103.4(4) 
            O(1)-C(31)-H(31A)           111.1 
            C(32)-C(31)-H(31A)          111.1 
            O(1)-C(31)-H(31B)           111.1 
            C(32)-C(31)-H(31B)          111.1 
            H(31A)-C(31)-H(31B)         109.1 
            C(33)-C(32)-C(31)           104.7(4) 
            C(33)-C(32)-H(32A)          110.8 
            C(31)-C(32)-H(32A)          110.8 
            C(33)-C(32)-H(32B)          110.8 
            C(31)-C(32)-H(32B)          110.8 
            H(32A)-C(32)-H(32B)         108.9 
            C(32)-C(33)-C(34)           106.3(4) 
            C(32)-C(33)-H(33A)          110.5 
            C(34)-C(33)-H(33A)          110.5 
            C(32)-C(33)-H(33B)          110.5 
            C(34)-C(33)-H(33B)          110.5 
            H(33A)-C(33)-H(33B)         108.7 
            O(1)-C(34)-C(33)            106.3(4) 
            O(1)-C(34)-H(34A)           110.5 
            C(33)-C(34)-H(34A)          110.5 
            O(1)-C(34)-H(34B)           110.5 
            C(33)-C(34)-H(34B)          110.5 
            H(34A)-C(34)-H(34B)         108.7 
            C(36)-C(35)-O(2)            105.1(4) 
            C(36)-C(35)-H(35A)          110.7 
            O(2)-C(35)-H(35A)           110.7 
            C(36)-C(35)-H(35B)          110.7 
            O(2)-C(35)-H(35B)           110.7 
            H(35A)-C(35)-H(35B)         108.8 
            C(37)-C(36)-C(35)           104.9(4) 
            C(37)-C(36)-H(36A)          110.8 
            C(35)-C(36)-H(36A)          110.8 
            C(37)-C(36)-H(36B)          110.8 
            C(35)-C(36)-H(36B)          110.8 
            H(36A)-C(36)-H(36B)         108.8 
            C(38)-C(37)-C(36)           105.6(5) 
            C(38)-C(37)-H(37A)          110.6 
            C(36)-C(37)-H(37A)          110.6 
            C(38)-C(37)-H(37B)          110.6 
            C(36)-C(37)-H(37B)          110.6 
            H(37A)-C(37)-H(37B)         108.8 
            O(2)-C(38)-C(37)            107.4(4) 
            O(2)-C(38)-H(38A)           110.2 
            C(37)-C(38)-H(38A)          110.2 
            O(2)-C(38)-H(38B)           110.2 
            C(37)-C(38)-H(38B)          110.2 
            H(38A)-C(38)-H(38B)         108.5 
           _____________________________________________________________ 
  
           Symmetry transformations used to generate equivalent atoms: 
            
  
    Table 4.  Anisotropic displacement parameters (A^2 x 10^3) for bas07. 
    The anisotropic displacement factor exponent takes the form: 
    -2 pi^2 [ h^2 a*^2 U11 + ... + 2 h k a* b* U12 ] 
  
    _______________________________________________________________________ 
  
              U11        U22        U33        U23        U13        U12 
    _______________________________________________________________________ 
  
    Cr(1)    41(1)      27(1)      26(1)      10(1)       5(1)      -2(1) 
    Cl(1)    58(1)      35(1)      37(1)       6(1)       3(1)     -11(1) 
    Cl(2)    70(1)      37(1)      38(1)      20(1)       2(1)      -8(1) 
    O(1)     48(1)      32(2)      39(1)      11(1)      10(1)       6(1) 
    O(2)     47(1)      32(2)      41(1)      13(1)      17(1)      -4(1) 
    N(1)     35(1)      28(2)      23(1)       9(1)       5(1)       1(1) 
    N(2)     34(1)      25(2)      26(1)       8(1)       6(1)       1(1) 
    N(3)     45(2)      33(2)      31(2)      14(1)       4(1)      -3(1) 
    C(1)     47(2)      24(2)      24(2)       8(2)       2(1)      -4(2) 
    C(2)     55(2)      31(3)      31(2)      12(2)       8(1)       3(2) 
    C(3)     70(3)      51(3)      32(2)      15(2)      14(2)      10(2) 
    C(4)     76(3)      62(3)      28(2)      13(2)      -9(2)      -1(2) 
    C(5)     51(2)      64(3)      38(2)      18(2)      -5(2)      -4(2) 
    C(6)     44(2)      46(3)      38(2)      17(2)       1(2)       0(2) 
    C(7)     43(2)      84(4)      44(2)      26(2)       5(2)       6(2) 
    C(8)     78(3)      95(5)      78(4)      22(3)      28(3)      25(3) 
    C(9)     53(3)     132(6)      75(3)      45(4)       8(2)     -13(3) 
    C(10)    56(2)      47(3)      34(2)      15(2)      16(2)       8(2) 
    C(11)    75(3)      64(4)      62(3)      13(3)      24(2)      21(3) 
    C(12)    64(3)      52(3)      57(3)      16(2)      17(2)      -3(2) 
    C(13)    38(2)      30(2)      30(2)      15(2)       7(1)       3(2) 
    C(14)    34(2)      30(2)      29(2)      13(2)       9(1)       0(1) 
    C(15)    43(2)      26(2)      36(2)      13(2)       8(1)      -4(2) 
    C(16)    46(2)      29(3)      29(2)       5(2)       6(1)      -3(2) 
    C(17)    36(2)      27(2)      27(2)       9(2)       7(1)      -1(1) 
    C(18)    40(2)      28(2)      30(2)      10(2)       8(1)       0(1) 
    C(19)    48(2)      21(2)      25(2)       6(2)       5(1)       0(2) 
    C(20)    50(2)      32(3)      35(2)      12(2)      11(1)       5(2) 
    C(21)    50(2)      56(3)      47(2)      28(2)       7(2)       9(2) 
    C(22)    63(2)      54(3)      45(2)      29(2)      11(2)      11(2) 
    C(23)    58(2)      54(3)      40(2)      24(2)      19(2)       5(2) 
    C(24)    48(2)      34(3)      34(2)      12(2)      12(1)       2(2) 
    C(25)    54(2)      40(3)      55(2)      24(2)      16(2)       4(2) 
    C(26)   101(4)      69(4)      95(4)      35(3)      65(3)      13(3) 
    C(27)    57(3)     111(5)      82(4)      43(4)       7(2)     -19(3) 
    C(28)    48(2)      85(4)      57(3)      43(3)      19(2)       9(2) 
    C(29)    61(3)     109(6)     105(4)      27(4)      13(3)     -20(3) 
    C(30)    92(4)     111(5)     101(5)      28(4)      40(3)      58(4) 
    C(31)    42(2)      51(3)      71(3)       8(2)      13(2)       1(2) 
    C(32)    57(3)      97(5)      84(4)      32(4)      23(2)      31(3) 
    C(33)    83(4)      79(5)     102(5)     -13(3)     -21(3)      46(3) 
    C(34)    86(3)      34(3)      68(3)       7(2)      21(2)      20(2) 
    C(35)    52(2)      48(3)      64(3)      20(2)      22(2)     -10(2) 
    C(36)    89(4)      74(5)      84(4)       6(3)      46(3)     -24(3) 
    C(37)   126(5)      63(5)     170(7)      26(5)     112(5)      10(4) 
    C(38)    74(3)      41(4)      86(3)      11(3)      48(2)       3(2) 
    _______________________________________________________________________ 
  
         Table 5.  Hydrogen coordinates ( x 10^4) and isotropic 
         displacement parameters (A^2 x 10^3) for bas07. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          H(3A)        8299          3677          5209          61 
          H(4A)       10411          3638          5716          72 
          H(5A)       11555          3192          4626          65 
          H(7A)       10390          2544          2109          69 
          H(8A)       10538           742          2370         126 
          H(8B)       11760          1307          3225         126 
          H(8C)       11786          1148          2168         126 
          H(9A)       11805          4253          3077         130 
          H(9B)       12520          3256          2557         130 
          H(9C)       12586          3513          3644         130 
          H(10A)       6505          3213          2835          54 
          H(11A)       6820          4985          4163         102 
          H(11B)       6465          4227          4764         102 
          H(11C)       5452          4293          3866         102 
          H(12A)       6148          1395          2956          88 
          H(12B)       5127          2141          3317          88 
          H(12C)       6286          1955          4063          88 
          H(13A)       7870           857          2066          38 
          H(15A)       6630          -927           256          42 
          H(16A)       5712          -772         -1360          44 
          H(18A)       6048          2399         -1282          40 
          H(21A)       2357          2028         -4265          60 
          H(22A)       3806          2786         -4848          62 
          H(23A)       5881          2622         -4331          57 
          H(25A)       3042           390         -2692          57 
          H(26A)       3156          2320         -1643         119 
          H(26B)       1872          1531         -1832         119 
          H(26C)       1930          2485         -2340         119 
          H(27A)       1647          -244         -4240         127 
          H(27B)        985           899         -3931         127 
          H(27C)        939           -78         -3442         127 
          H(28A)       7250          1351         -2572          69 
          H(29A)       8802          2812         -2427         145 
          H(29B)       7692          3423         -2091         145 
          H(29C)       7851          3313         -3108         145 
          H(30A)       8304           718         -3691         149 
          H(30B)       7563          1399         -4333         149 
          H(30C)       6881           257         -4253         149 
          H(31A)       5012          2475           866          70 
          H(31B)       4948          3383           294          70 
          H(32A)       3458          3949          1047          94 
          H(32B)       4172          3655          1963          94 
          H(33A)       4809          5579          2555         127 
          H(33B)       4597          5696          1528         127 
          H(34A)       6570          5648          1669          78 
          H(34B)       6756          5414          2653          78 
          H(35A)       9959          4332           425          65 
          H(35B)      11013          3943          1132          65 
          H(36A)      10298          3067          -855         102 
          H(36B)      11656          3219          -153         102 
          H(37A)      10381          1189          -976         132 
          H(37B)      11272          1527            80         132 
          H(38A)       8712          1329          -500          78 
          H(38B)       9564          1109           407          78 
         ________________________________________________________________ 
  
         Table 6.  Torsion angles [deg] for bas07. 
         ________________________________________________________________ 
  
          O(2)-Cr(1)-O(1)-C(31)                                33.4(17) 
          N(2)-Cr(1)-O(1)-C(31)                               -21.4(3) 
          N(1)-Cr(1)-O(1)-C(31)                              -102.3(3) 
          Cl(1)-Cr(1)-O(1)-C(31)                              169.5(3) 
          Cl(2)-Cr(1)-O(1)-C(31)                               75.4(3) 
          O(2)-Cr(1)-O(1)-C(34)                              -110.4(15) 
          N(2)-Cr(1)-O(1)-C(34)                              -165.2(3) 
          N(1)-Cr(1)-O(1)-C(34)                               113.9(3) 
          Cl(1)-Cr(1)-O(1)-C(34)                               25.7(3) 
          Cl(2)-Cr(1)-O(1)-C(34)                              -68.4(3) 
          O(1)-Cr(1)-O(2)-C(38)                               -62.6(16) 
          N(2)-Cr(1)-O(2)-C(38)                                -7.7(3) 
          N(1)-Cr(1)-O(2)-C(38)                                73.0(3) 
          Cl(1)-Cr(1)-O(2)-C(38)                              161.3(3) 
          Cl(2)-Cr(1)-O(2)-C(38)                             -104.5(3) 
          O(1)-Cr(1)-O(2)-C(35)                                95.1(16) 
          N(2)-Cr(1)-O(2)-C(35)                               150.0(3) 
          N(1)-Cr(1)-O(2)-C(35)                              -129.2(3) 
          Cl(1)-Cr(1)-O(2)-C(35)                              -41.0(2) 
          Cl(2)-Cr(1)-O(2)-C(35)                               53.2(2) 
          O(1)-Cr(1)-N(1)-C(13)                                96.0(2) 
          O(2)-Cr(1)-N(1)-C(13)                               -81.4(2) 
          N(2)-Cr(1)-N(1)-C(13)                                 5.1(2) 
          Cl(1)-Cr(1)-N(1)-C(13)                             -171.5(2) 
          Cl(2)-Cr(1)-N(1)-C(13)                               52.2(16) 
          O(1)-Cr(1)-N(1)-C(1)                                -84.3(3) 
          O(2)-Cr(1)-N(1)-C(1)                                 98.3(3) 
          N(2)-Cr(1)-N(1)-C(1)                               -175.2(3) 
          Cl(1)-Cr(1)-N(1)-C(1)                                 8.2(3) 
          Cl(2)-Cr(1)-N(1)-C(1)                              -128.1(14) 
          O(1)-Cr(1)-N(2)-C(17)                                98.7(4) 
          O(2)-Cr(1)-N(2)-C(17)                               -78.1(4) 
          N(1)-Cr(1)-N(2)-C(17)                              -171.5(4) 
          Cl(1)-Cr(1)-N(2)-C(17)                             -154.0(3) 
          Cl(2)-Cr(1)-N(2)-C(17)                               11.0(4) 
          O(1)-Cr(1)-N(2)-C(14)                               -96.4(2) 
          O(2)-Cr(1)-N(2)-C(14)                                86.7(2) 
          N(1)-Cr(1)-N(2)-C(14)                                -6.7(2) 
          Cl(1)-Cr(1)-N(2)-C(14)                               10.9(6) 
          Cl(2)-Cr(1)-N(2)-C(14)                              175.8(2) 
          C(13)-N(1)-C(1)-C(2)                                -84.2(4) 
          Cr(1)-N(1)-C(1)-C(2)                                 96.1(4) 
          C(13)-N(1)-C(1)-C(6)                                 92.9(4) 
          Cr(1)-N(1)-C(1)-C(6)                                -86.8(4) 
          C(6)-C(1)-C(2)-C(3)                                  -1.7(6) 
          N(1)-C(1)-C(2)-C(3)                                 175.3(3) 
          C(6)-C(1)-C(2)-C(10)                                179.6(4) 
          N(1)-C(1)-C(2)-C(10)                                 -3.3(5) 
          C(1)-C(2)-C(3)-C(4)                                   0.0(6) 
          C(10)-C(2)-C(3)-C(4)                                178.7(4) 
          C(2)-C(3)-C(4)-C(5)                                   1.5(7) 
          C(3)-C(4)-C(5)-C(6)                                  -1.3(7) 
          C(4)-C(5)-C(6)-C(1)                                  -0.4(6) 
          C(4)-C(5)-C(6)-C(7)                                -178.6(4) 
          C(2)-C(1)-C(6)-C(5)                                   1.9(6) 
          N(1)-C(1)-C(6)-C(5)                                -175.2(4) 
          C(2)-C(1)-C(6)-C(7)                                -179.9(4) 
          N(1)-C(1)-C(6)-C(7)                                   3.0(6) 
          C(5)-C(6)-C(7)-C(8)                                  73.4(5) 
          C(1)-C(6)-C(7)-C(8)                                -104.7(4) 
          C(5)-C(6)-C(7)-C(9)                                 -50.5(6) 
          C(1)-C(6)-C(7)-C(9)                                 131.4(4) 
          C(1)-C(2)-C(10)-C(12)                                98.5(4) 
          C(3)-C(2)-C(10)-C(12)                               -80.2(5) 
          C(1)-C(2)-C(10)-C(11)                              -136.9(4) 
          C(3)-C(2)-C(10)-C(11)                                44.5(5) 
          C(1)-N(1)-C(13)-C(14)                               177.8(3) 
          Cr(1)-N(1)-C(13)-C(14)                               -2.4(4) 
          C(17)-N(2)-C(14)-C(15)                                0.4(4) 
          Cr(1)-N(2)-C(14)-C(15)                             -170.4(2) 
          C(17)-N(2)-C(14)-C(13)                              178.4(3) 
          Cr(1)-N(2)-C(14)-C(13)                                7.7(3) 
          N(1)-C(13)-C(14)-N(2)                                -3.6(5) 
          N(1)-C(13)-C(14)-C(15)                              173.9(4) 
          N(2)-C(14)-C(15)-C(16)                                0.1(4) 
          C(13)-C(14)-C(15)-C(16)                            -177.6(3) 
          C(14)-C(15)-C(16)-C(17)                              -0.4(4) 
          C(15)-C(16)-C(17)-N(2)                                0.7(4) 
          C(15)-C(16)-C(17)-C(18)                            -177.3(3) 
          C(14)-N(2)-C(17)-C(16)                               -0.6(4) 
          Cr(1)-N(2)-C(17)-C(16)                              164.6(3) 
          C(14)-N(2)-C(17)-C(18)                              177.4(3) 
          Cr(1)-N(2)-C(17)-C(18)                              -17.3(6) 
          C(19)-N(3)-C(18)-C(17)                             -177.8(3) 
          C(16)-C(17)-C(18)-N(3)                                1.4(5) 
          N(2)-C(17)-C(18)-N(3)                              -176.3(3) 
          C(18)-N(3)-C(19)-C(24)                               71.1(5) 
          C(18)-N(3)-C(19)-C(20)                             -113.5(4) 
          C(24)-C(19)-C(20)-C(21)                              -3.3(6) 
          N(3)-C(19)-C(20)-C(21)                             -178.7(4) 
          C(24)-C(19)-C(20)-C(25)                             176.8(4) 
          N(3)-C(19)-C(20)-C(25)                                1.5(5) 
          C(19)-C(20)-C(21)-C(22)                               1.2(6) 
          C(25)-C(20)-C(21)-C(22)                            -179.0(4) 
          C(20)-C(21)-C(22)-C(23)                               1.8(7) 
          C(21)-C(22)-C(23)-C(24)                              -2.7(7) 
          C(20)-C(19)-C(24)-C(23)                               2.5(6) 
          N(3)-C(19)-C(24)-C(23)                              177.7(3) 
          C(20)-C(19)-C(24)-C(28)                            -173.6(4) 
          N(3)-C(19)-C(24)-C(28)                                1.6(6) 
          C(22)-C(23)-C(24)-C(19)                               0.5(6) 
          C(22)-C(23)-C(24)-C(28)                             176.7(4) 
          C(21)-C(20)-C(25)-C(26)                             -88.4(5) 
          C(19)-C(20)-C(25)-C(26)                              91.4(5) 
          C(21)-C(20)-C(25)-C(27)                              38.5(6) 
          C(19)-C(20)-C(25)-C(27)                            -141.6(4) 
          C(19)-C(24)-C(28)-C(29)                            -120.1(5) 
          C(23)-C(24)-C(28)-C(29)                              63.9(5) 
          C(19)-C(24)-C(28)-C(30)                             117.0(5) 
          C(23)-C(24)-C(28)-C(30)                             -58.9(6) 
          C(34)-O(1)-C(31)-C(32)                              -31.3(5) 
          Cr(1)-O(1)-C(31)-C(32)                             -179.6(3) 
          O(1)-C(31)-C(32)-C(33)                               33.7(5) 
          C(31)-C(32)-C(33)-C(34)                             -23.6(6) 
          C(31)-O(1)-C(34)-C(33)                               17.0(5) 
          Cr(1)-O(1)-C(34)-C(33)                              165.0(3) 
          C(32)-C(33)-C(34)-O(1)                                4.8(6) 
          C(38)-O(2)-C(35)-C(36)                               12.4(5) 
          Cr(1)-O(2)-C(35)-C(36)                             -149.1(3) 
          O(2)-C(35)-C(36)-C(37)                              -26.0(6) 
          C(35)-C(36)-C(37)-C(38)                              30.2(7) 
          C(35)-O(2)-C(38)-C(37)                                6.4(6) 
          Cr(1)-O(2)-C(38)-C(37)                              166.6(4) 
          C(36)-C(37)-C(38)-O(2)                              -22.8(7) 
         ________________________________________________________________ 
  
         Symmetry transformations used to generate equivalent atoms: 
          
  
