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3.20066 5 1 -2 11 28.7645 1.91566 5 1 -2 11 27.6566 1.91202 16 -1 -2 -11 27.2115 2.02097 5 -1 -2 -11 29.2532 1.99634 8 -1 -2 -11 26.4578 1.96344 13 -1 2 -11 27.9333 1.97866 8 1 2 11 29.3187 1.96391 5 1 2 11 24.0447 1.92190 13 -1 2 -11 28.2381 1.96922 5 -2 -2 -11 0.50434 0.40453 8 5 -3 -11 25.5889 1.68971 13 5 3 -11 23.4175 1.68658 16 4 -3 -11 7.77534 0.77231 2 4 -3 -11 5.23429 0.70775 13 4 -3 -11 6.90920 0.69072 5 4 -3 -11 6.87994 0.67229 9 4 -3 -11 6.83568 0.72179 14 4 3 -11 7.02111 0.68683 3 4 3 -11 7.03220 0.73106 14 4 3 -11 8.03820 0.76162 16 4 3 -11 8.25358 0.78646 5 4 3 -11 7.56289 0.70646 2 4 3 -11 7.97013 0.70928 9 3 -3 -11 4.86168 0.73644 3 3 -3 -11 6.30691 0.75081 9 3 -3 -11 5.51685 0.69734 5 3 -3 -11 6.45859 0.77428 13 3 -3 -11 6.47887 0.79794 2 -3 -3 11 7.17655 0.73215 16 3 3 -11 7.17242 0.77472 3 3 3 -11 5.39375 0.69724 14 3 3 -11 5.99856 0.74803 16 3 3 -11 5.69308 0.71446 5 2 -3 -11 40.7534 2.82808 3 -2 -3 11 42.5594 2.80535 16 2 -3 -11 39.4906 2.75505 14 2 -3 -11 37.8733 2.73263 5 2 -3 -11 43.5928 2.86839 2 2 -3 -11 35.7760 2.76028 13 2 -3 -11 41.4307 2.72430 9 2 -3 -11 37.5826 2.60554 15 2 3 -11 38.0077 2.59958 15 2 3 -11 39.7287 2.73581 5 2 3 -11 38.0462 2.73821 3 2 3 -11 39.3342 2.68525 9 2 3 -11 38.1762 2.85191 16 1 -3 -11 0.61498 0.48969 9 1 -3 -11 0.33711 0.44975 3 1 -3 -11 0.41501 0.46031 2 1 -3 -11 0.36963 0.47953 13 -1 -3 11 0.38216 0.41661 16 1 -3 -11 0.20094 0.27595 15 1 -3 -11 0.08126 0.38735 14 1 -3 -11 0.66740 0.43422 5 1 -3 -11 0.20262 0.42329 8 -1 -3 11 -0.1281 0.36988 5 1 3 -11 0.73460 0.42545 5 1 3 -11 0.46983 0.50189 16 1 3 -11 0.45283 0.42703 3 0 -3 -11 0.84389 0.42244 13 0 -3 -11 0.62685 0.26039 9 0 -3 -11 0.44706 0.38756 8 0 -3 11 0.51803 0.28706 5 0 -3 -11 0.68564 0.39522 5 0 -3 -11 0.44695 0.38288 2 0 -3 -11 0.11137 0.28965 15 0 -3 -11 0.75858 0.33754 3 0 -3 11 0.55233 0.33757 16 0 3 -11 0.40272 0.37315 8 0 3 11 0.33937 0.31860 5 0 3 -11 0.86319 0.36300 5 0 3 -11 0.74813 0.40750 16 0 3 -11 0.90479 0.44284 3 1 -3 11 0.28299 0.27828 16 -1 -3 -11 0.51415 0.35360 8 -1 -3 -11 0.60743 0.35710 13 1 -3 11 0.58386 0.22848 5 -1 -3 -11 0.80412 0.32103 5 -1 3 -11 0.66956 0.33654 8 -1 3 -11 0.59909 0.27335 5 1 3 11 0.60531 0.26800 5 1 3 11 0.51176 0.33721 13 4 -4 -11 0.38526 0.28207 13 4 -4 -11 0.31583 0.27395 2 4 -4 -11 0.31619 0.25465 9 4 -4 -11 0.56698 0.31915 5 -4 -4 11 0.49310 0.30308 16 4 4 -11 0.00958 0.26193 9 4 4 -11 0.26371 0.31344 16 4 4 -11 0.19657 0.24274 3 3 -4 -11 0.03276 0.27882 5 3 -4 -11 0.69810 0.47524 3 3 -4 -11 0.20369 0.38327 14 3 -4 -11 0.18769 0.35740 2 3 -4 -11 -0.0124 0.33510 9 3 -4 -11 -0.0247 0.33588 13 -3 -4 11 -0.1476 0.34827 16 3 4 -11 0.03842 0.37285 16 3 4 -11 0.00868 0.33855 3 3 4 -11 0.19461 0.30287 9 3 4 -11 0.46137 0.44748 14 2 -4 -11 0.77722 0.24270 15 2 -4 -11 1.52280 0.37824 5 -2 -4 11 1.80061 0.42189 16 2 -4 -11 1.08968 0.44031 2 2 -4 -11 0.82127 0.43062 14 2 -4 -11 1.18558 0.44203 13 2 -4 -11 0.97672 0.40948 3 2 -4 -11 1.41391 0.36509 9 2 4 -11 1.93469 0.42666 3 2 4 -11 1.34579 0.45824 16 2 4 -11 1.24525 0.32616 9 2 4 -11 1.61135 0.26112 15 1 -4 -11 43.7123 3.01292 13 1 -4 -11 43.4907 2.86262 15 1 -4 -11 44.2482 2.99780 2 1 -4 -11 43.6922 2.97992 14 1 -4 -11 44.1485 2.92832 9 1 -4 -11 41.8881 2.97582 5 1 -4 -11 42.6013 2.98359 8 1 -4 -11 44.3014 2.97427 3 -1 4 11 41.4924 2.92259 5 1 4 -11 46.2518 2.97752 3 0 -4 -11 19.8036 1.45090 15 0 -4 -11 20.3813 1.59583 2 0 -4 -11 23.0665 1.63434 13 0 -4 -11 19.9210 1.52562 3 0 -4 -11 21.0657 1.58348 5 0 -4 11 22.9516 1.56281 16 0 -4 -11 21.1806 1.49522 9 0 4 -11 21.2703 1.55192 8 0 4 -11 22.5855 1.46006 15 0 4 11 21.4863 1.52975 5 -1 -4 -11 2.94144 0.42944 13 -1 -4 -11 3.51949 0.46188 8 1 4 11 1.86405 0.35444 13 -1 4 -11 3.52855 0.45615 8 -4 -5 11 25.4336 1.65400 16 4 -5 -11 23.4549 1.67010 2 4 5 -11 22.2713 1.66245 16 4 5 -11 25.9685 1.66670 9 -3 -5 11 2.38987 0.38227 16 3 -5 -11 2.73879 0.42414 2 3 -5 -11 3.31703 0.50181 9 3 -5 -11 3.24771 0.46872 14 3 -5 -11 1.79409 0.46606 13 3 -5 -11 2.73860 0.40865 3 3 5 -11 2.58723 0.39974 3 3 5 -11 2.66147 0.43345 16 3 5 -11 2.47980 0.36881 9 2 -5 -11 0.41980 0.30521 9 2 -5 -11 0.59810 0.20131 15 2 -5 -11 0.29825 0.34029 2 2 -5 -11 0.07730 0.31512 13 2 -5 -11 0.31162 0.45366 3 2 -5 -11 0.13247 0.34920 14 -2 -5 11 1.03216 0.34958 16 2 5 -11 0.70884 0.37563 3 2 5 -11 0.10477 0.16954 15 2 5 -11 0.35180 0.36960 16 2 5 -11 0.32579 0.24228 9 -1 -5 11 7.15659 0.74349 16 1 -5 -11 8.63366 0.80312 13 1 -5 -11 5.78232 0.71393 14 1 -5 -11 7.82224 0.63080 15 1 -5 -11 8.19290 0.80897 2 1 -5 -11 9.40557 0.78782 3 1 -5 -11 8.21815 0.77039 8 1 5 -11 7.54169 0.74334 3 1 5 -11 8.04330 0.63478 15 1 5 -11 6.27284 0.79508 16 0 -5 -11 25.1151 1.73334 2 0 -5 -11 23.2594 1.66413 3 0 -5 11 23.4422 1.67822 16 0 -5 -11 24.8017 1.74074 13 0 -5 -11 21.3921 1.62204 9 0 5 11 25.9030 1.71798 13 0 5 -11 24.2966 1.67611 8 -1 -5 -11 1.13713 0.30963 13 1 -5 11 1.06232 0.44330 16 -1 -5 -11 1.62636 0.37254 8 1 5 11 1.60888 0.40463 13 3 -6 -11 -0.3408 0.41376 3 3 -6 -11 0.20069 0.32593 2 -3 -6 11 0.24217 0.22323 16 3 -6 -11 0.03739 0.24459 9 3 6 -11 -0.1367 0.21958 16 3 6 -11 0.13245 0.25051 3 3 6 -11 0.17756 0.29041 9 -2 -6 11 2.03851 0.33365 16 2 -6 -11 0.99324 0.32220 2 2 -6 -11 1.68424 0.32311 9 2 -6 -11 1.60978 0.31786 13 2 -6 -11 2.04523 0.35655 3 2 6 -11 2.45394 0.39926 3 2 6 -11 1.46944 0.34154 16 -1 -6 11 3.90434 0.46146 16 1 -6 -11 2.64077 0.37247 9 1 -6 -11 3.22198 0.41742 13 1 -6 -11 3.41179 0.48949 8 1 -6 -11 3.46608 0.49166 3 1 -6 -11 2.83480 0.45468 2 1 6 -11 3.90334 0.47709 3 0 -6 -11 4.64853 0.52032 8 0 -6 -11 4.09574 0.49900 2 0 -6 -11 4.52514 0.50701 13 0 -6 11 2.88377 0.47439 16 0 6 11 4.82208 0.47055 13 3 0 -12 14.7615 1.04842 9 3 0 -12 13.0253 1.06526 13 3 0 -12 11.4742 1.00222 16 3 0 -12 14.6849 1.03565 5 -3 0 12 15.0436 1.07221 16 3 0 -12 13.3933 1.05792 3 3 0 -12 13.6821 1.01555 2 -2 0 12 74.0787 4.85955 16 2 0 -12 78.5309 4.86719 9 2 0 -12 76.3702 4.89871 13 2 0 -12 78.8623 4.92817 5 2 0 -12 78.7844 4.89654 3 2 0 -12 65.2419 4.86271 16 1 0 -12 3.06247 0.41301 3 -1 0 12 1.96504 0.29400 5 1 0 -12 1.65701 0.34127 5 1 0 -12 1.04702 0.32944 13 -3 -1 12 41.6663 2.96383 16 3 -1 -12 47.9215 3.01046 2 3 -1 -12 42.4294 2.97027 9 3 -1 -12 45.5401 2.99060 3 3 -1 -12 44.2496 2.99651 5 3 -1 -12 44.8770 3.00963 13 3 1 -12 47.7909 2.97560 9 3 1 -12 43.9890 2.97562 3 3 1 -12 49.6169 3.02108 5 2 -1 -12 49.2620 3.17899 13 -2 -1 12 50.3652 3.15921 16 2 -1 -12 46.2877 3.16504 5 2 -1 -12 47.5918 3.16887 2 2 -1 -12 46.3029 3.15267 3 -2 -1 12 51.0117 3.15384 5 2 -1 -12 49.8845 3.15190 9 2 1 -12 46.2328 3.16704 5 2 1 -12 41.8462 3.10971 9 2 1 -12 45.8850 3.15885 3 -2 1 12 51.0696 3.15477 5 -1 -1 12 10.8719 0.76627 5 1 -1 -12 8.28524 0.77903 5 -1 -1 12 9.66888 0.74291 16 1 -1 -12 9.65359 0.79357 13 1 -1 -12 10.7504 0.85024 3 1 1 -12 9.79899 0.77297 3 -1 1 12 7.40659 0.73562 5 1 1 -12 10.9016 0.80679 5 3 -2 -12 16.4290 1.14074 2 3 -2 -12 16.5969 1.16522 13 -3 -2 12 17.1183 1.13659 16 3 -2 -12 14.7195 1.16296 9 3 2 -12 13.8454 1.14039 16 3 2 -12 15.6515 1.11288 9 2 -2 -12 10.2972 0.88884 2 2 -2 -12 10.5258 0.82605 3 2 -2 -12 10.2084 0.81378 5 2 -2 -12 10.9836 0.84701 9 -2 -2 12 10.2515 0.78812 5 -2 -2 12 10.5942 0.79911 16 2 2 -12 9.05104 0.81348 16 2 2 -12 8.93558 0.80720 5 -2 2 12 10.5112 0.79141 5 2 2 -12 10.7622 0.82507 3 -1 -2 12 -0.0761 0.18373 5 1 -2 -12 0.03820 0.33759 13 1 -2 -12 0.03377 0.31403 3 -1 -2 12 0.05027 0.19391 16 1 -2 -12 0.12372 0.33160 5 -1 2 12 -0.0595 0.29167 5 1 2 -12 0.02467 0.31813 3 1 2 -12 0.13679 0.23720 5 2 -3 -12 34.3037 2.10437 2 -2 -3 12 30.4805 2.04649 16 2 -3 -12 31.8082 2.07868 13 2 -3 -12 29.2455 2.04741 3 2 -3 -12 31.7053 2.04535 9 2 3 -12 26.5384 2.05341 16 2 3 -12 30.4010 2.05666 3 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7539 _exptl_absorpt_correction_T_min 0.5137 _exptl_special_details ; The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54185 7.083 12.730 9.816 89.992 102.319 89.980 ;