data_mils028
_publ_section_references          
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;

_cell_measurement_reflns_used     9614
_cell_measurement_temperature     200.00
_cell_measurement_theta_max       74.511
_cell_measurement_theta_min       3.404
_exptl_absorpt_correction_T_max   0.7538
_exptl_absorpt_correction_T_min   0.6220
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_process_details    
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1074 before and 0.0603 after correction.
The Ratio of minimum to maximum transmission is 0.8252.
The \l/2 correction factor is Not present.
;

_exptl_crystal_colour             orange
_exptl_crystal_colour_primary     orange
_exptl_crystal_description        plate
_exptl_crystal_F_000              1644
loop_
  _exptl_crystal_face_index_h
  _exptl_crystal_face_index_k
  _exptl_crystal_face_index_l
  _exptl_crystal_face_perp_dist
  -3.00   0.00  -1.00  0.0470
  -2.00   1.00   0.00  0.0230
  -2.00   1.00   3.00  0.0600
  -2.00   3.00   0.00  0.0250
  -2.00  -3.00  -1.00  0.0980
  -1.00   0.00   2.00  0.0930
  -1.00   0.00  -3.00  0.0730
  -1.00   3.00  -1.00  0.0280
   0.00   0.00  -1.00  0.0790
   0.00   0.00   1.00  0.1000
   0.00   3.00  -1.00  0.0450
   1.00  -3.00   1.00  0.0810
   1.00  -2.00  -2.00  0.0890
   2.00  -1.00   0.00  0.0820
   2.00  -1.00  -3.00  0.0980
   2.00   2.00  -3.00  0.0850
   2.00   3.00   1.00  0.0790
   2.00   2.00   3.00  0.0900
   2.00   1.00  -1.00  0.0850
   3.00   0.00  -1.00  0.0770
   3.00  -3.00  -1.00  0.0600

_exptl_crystal_size_max           0.237
_exptl_crystal_size_mid           0.187
_exptl_crystal_size_min           0.122
_diffrn_measurement_device_type   'Bruker Venture Photon III'
_diffrn_measurement_method        '\f and \w scans'
_computing_cell_refinement        'SAINT V8.42 (?, 2016)'
_computing_data_reduction         'SAINT V8.42 (?, 2016)'
_computing_molecular_graphics     'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material   'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement   'SHELXL 2019/3 (Sheldrick, 2015)'
_computing_structure_solution     'SHELXT 2018/2 (Sheldrick, 2018)'
_olex2_submission_special_instructions 'No special instructions were received'
_audit_creation_date              2026-04-10
_audit_creation_method            
;
Olex2 1.5
(compiled 2026.03.20 svn.r2bc28608 for OlexSys, GUI svn.r7524)
;

_publ_contact_author_email        ?
_publ_contact_author_phone        ?
_publ_contact_author_address      ?
_publ_contact_author_id_orcid     ?
_publ_contact_author_name         ''