data_rudi004
_audit_creation_date               2026-04-09
_audit_creation_method
;
Olex2 1.5
(compiled 2026.04.07 svn.r39635298 for OlexSys, GUI svn.r7533)
;
_shelx_SHELXL_version_number       '2019/3'
_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
D. Kratzert, I. Krossing, (2018), J. Appl. Cryst. 51, 928-934.

Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Kratzert, D., Holstein, J.J. & Krossing, I. (2015). J. Appl. Cryst. 48, 933-938.

Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic          ?
_chemical_formula_moiety           'C14 H16 Ni, 2(C H B11 Cl11), 2(C7 H8)'
_chemical_formula_sum              'C30 H34 B22 Cl22 Ni'
_chemical_formula_weight           1471.00
_chemical_melting_point            ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'B' 'B' 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Ni' 'Ni' -3.0029 0.5091
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'triclinic'
_space_group_IT_number             2
_space_group_name_H-M_alt          'P -1'
_space_group_name_Hall             '-P 1'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-x, -y, -z'

_cell_length_a                     11.9319(4)
_cell_length_b                     13.0302(4)
_cell_length_c                     19.2173(6)
_cell_angle_alpha                  93.964(2)
_cell_angle_beta                   98.5600(10)
_cell_angle_gamma                  97.1400(10)
_cell_volume                       2919.90(16)
_cell_formula_units_Z              2
_cell_measurement_reflns_used      9662
_cell_measurement_temperature      100.00
_cell_measurement_theta_max        74.401
_cell_measurement_theta_min        2.334
_shelx_estimated_absorpt_T_max     0.324
_shelx_estimated_absorpt_T_min     0.169
_exptl_absorpt_coefficient_mu      9.978
_exptl_absorpt_correction_T_max    0.7538
_exptl_absorpt_correction_T_min    0.3773
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1477 before and 0.0768 after correction.
The Ratio of minimum to maximum transmission is 0.5005.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details     ?
_exptl_crystal_colour              red
_exptl_crystal_colour_primary      red
_exptl_crystal_density_diffrn      1.673
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?
_exptl_crystal_description         plate
_exptl_crystal_F_000               1452
_exptl_crystal_size_max            0.276
_exptl_crystal_size_mid            0.233
_exptl_crystal_size_min            0.146
_exptl_transmission_factor_max     ?
_exptl_transmission_factor_min     ?
_diffrn_reflns_av_R_equivalents    0.0538
_diffrn_reflns_av_unetI/netI       0.0307
_diffrn_reflns_Laue_measured_fraction_full  0.996
_diffrn_reflns_Laue_measured_fraction_max  0.983
_diffrn_reflns_limit_h_max         14
_diffrn_reflns_limit_h_min         -14
_diffrn_reflns_limit_k_max         16
_diffrn_reflns_limit_k_min         -15
_diffrn_reflns_limit_l_max         23
_diffrn_reflns_limit_l_min         -23
_diffrn_reflns_number              93351
_diffrn_reflns_point_group_measured_fraction_full  0.996
_diffrn_reflns_point_group_measured_fraction_max  0.983
_diffrn_reflns_theta_full          67.679
_diffrn_reflns_theta_max           74.541
_diffrn_reflns_theta_min           2.334
_diffrn_ambient_temperature        100.00
_diffrn_detector_area_resol_mean   ?
_diffrn_measured_fraction_theta_full  0.996
_diffrn_measured_fraction_theta_max  0.983
_diffrn_measurement_device_type    'Bruker Photon III'
_diffrn_measurement_method         ?
_diffrn_radiation_type             CuK\a
_diffrn_radiation_wavelength       1.54178
_diffrn_source                     ?
_diffrn_source_current             1.2
_diffrn_source_power               0.06
_diffrn_source_voltage             50.0
_reflns_Friedel_coverage           0.000
_reflns_Friedel_fraction_full      .
_reflns_Friedel_fraction_max       .
_reflns_number_gt                  10546
_reflns_number_total               11733
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression       'I > 2σ(I)'
_computing_cell_refinement         'SAINT V8.42 (?, 2016)'
_computing_data_collection         ?
_computing_data_reduction          'SAINT V8.42 (?, 2016)'
_computing_molecular_graphics      'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement    'SHELXL 2019/3 (Sheldrick, 2015)'
_computing_structure_solution      'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max           0.914
_refine_diff_density_min           -0.691
_refine_diff_density_rms           0.102
_refine_ls_extinction_coef         .
_refine_ls_extinction_method       none
_refine_ls_goodness_of_fit_ref     1.033
_refine_ls_hydrogen_treatment      constr
_refine_ls_matrix_type             full
_refine_ls_number_parameters       745
_refine_ls_number_reflns           11733
_refine_ls_number_restraints       468
_refine_ls_R_factor_all            0.0442
_refine_ls_R_factor_gt             0.0385
_refine_ls_restrained_S_all        1.040
_refine_ls_shift/su_max            0.001
_refine_ls_shift/su_mean           0.000
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[σ²(Fo²)+(0.0595P)²+4.3069P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.0999
_refine_ls_wR_factor_ref           0.1038
_refine_special_details            ?
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C30-C29 = C30A-C29A
 1.51 with sigma of 0.02
 C29-C28 = C29-C24 = C27-C26 = C29A-C28A = C29A-C24A = C27A-C26A
 1.39 with sigma of 0.02
 C28-C27 = C26-C25 = C25-C24 = C28A-C27A = C26A-C25A = C25A-C24A
 1.38 with sigma of 0.02
 C30-C28 = C30-C24 = C30A-C28A = C30A-C24A
 2.52 with sigma of 0.04
 C29-C27 = C29A-C27A
 2.42 with sigma of 0.04
 C29-C25 = C29A-C25A
 2.41 with sigma of 0.04
 C28-C26 = C28A-C26A
 2.39 with sigma of 0.04
 C27-C25 = C26-C24 = C27A-C25A = C26A-C24A
 2.4 with sigma of 0.04
 C29-C28 \\sim C28-C27 \\sim C27-C26 \\sim C26-C25 \\sim C25-C24 \\sim C24-C29
\\sim C29A-C28A \\sim C28A-
 C27A \\sim C27A-C26A \\sim C26A-C25A \\sim C25A-C24A \\sim C24A-C29A
 with sigma of 0.02
 C29-C25 \\sim C29-C27 \\sim C24-C26 \\sim C28-C24 \\sim C27-C25 \\sim C28-C26
\\sim C29A-C25A \\sim C29A-
 C27A \\sim C24A-C26A \\sim C28A-C24A \\sim C27A-C25A \\sim C28A-C26A
 with sigma of 0.04
 C30-C24 \\sim C30-C28 \\sim C30A-C24A \\sim C30A-C28A
 with sigma of 0.04
3. Restrained planarity
 C24, C25, C26, C27, C28, C29, C30
 with sigma of 0.05
 C24A, C25A, C26A, C27A, C28A, C29A, C30A
 with sigma of 0.05
4. Uiso/Uaniso restraints and constraints
C24 \\sim C25 \\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim C30 \\sim C24A
\\sim C25A \\sim C26A \\sim C27A \\sim C28A \\sim C29A \\sim C30A: within 2A
with sigma of 0.002 and sigma for terminal atoms of 0.004 within 2A
5. Rigid body (RIGU) restrains
 C24, C25, C26, C27, C28, C29, C30, C24A, C25A, C26A, C27A, C28A, C29A, C30A
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
6. Others
 Sof(C24A)=Sof(H24A)=Sof(C25A)=Sof(H25A)=Sof(C26A)=Sof(H26A)=Sof(C27A)=
 Sof(H27A)=Sof(C28A)=Sof(H28A)=Sof(C29A)=Sof(C30A)=Sof(H30D)=Sof(H30E)=
 Sof(H30F)=1-FVAR(1)
 Sof(C24)=Sof(H24)=Sof(C25)=Sof(H25)=Sof(C26)=Sof(H26)=Sof(C27)=Sof(H27)=
 Sof(C28)=Sof(H28)=Sof(C29)=Sof(C30)=Sof(H30A)=Sof(H30B)=Sof(H30C)=FVAR(1)
7.a Aromatic/amide H refined with riding coordinates:
 C1(H1), C2(H2), C3(H3), C4(H4), C5(H5), C8(H8), C9(H9), C10(H10), C11(H11),
 C12(H12), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21), C24(H24), C25(H25),
  C26(H26), C27(H27), C28(H28), C24A(H24A), C25A(H25A), C26A(H26A), C27A(H27A),
 C28A(H28A)
7.b Idealised Me refined as rotating group:
 C7(H7A,H7B,H7C), C14(H14A,H14B,H14C), C23(H23A,H23B,H23C), C30(H30A,H30B,
 H30C), C30A(H30D,H30E,H30F)
7.c Boron cage BH refined with riding coordinates:
 C15(H15), C16(H16)
;
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary       dual
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 Ni1 Ni 0.75589(4) 0.38025(3) 0.75273(2) 0.01260(10) Uani 1 1 d . . . . .
 C1 C 0.5789(2) 0.42839(19) 0.74434(13) 0.0128(5) Uani 1 1 d . . . . .
 H1 H 0.509571 0.393173 0.717783 0.015 Uiso 1 1 calc R U . . .
 C2 C 0.6463(2) 0.50131(19) 0.71271(14) 0.0143(5) Uani 1 1 d . . . . .
 H2 H 0.622396 0.515356 0.665336 0.017 Uiso 1 1 calc R U . . .
 C3 C 0.7496(2) 0.55390(19) 0.75093(14) 0.0143(5) Uani 1 1 d . . . . .
 H3 H 0.795452 0.603890 0.729791 0.017 Uiso 1 1 calc R U . . .
 C4 C 0.7842(2) 0.5315(2) 0.82091(14) 0.0148(5) Uani 1 1 d . . . . .
 H4 H 0.854018 0.566449 0.847055 0.018 Uiso 1 1 calc R U . . .
 C5 C 0.7164(2) 0.4581(2) 0.85229(13) 0.0141(5) Uani 1 1 d . . . . .
 H5 H 0.741359 0.443263 0.899351 0.017 Uiso 1 1 calc R U . . .
 C6 C 0.6112(2) 0.40576(19) 0.81479(13) 0.0125(5) Uani 1 1 d . . . . .
 C7 C 0.5367(2) 0.3295(2) 0.84801(14) 0.0176(6) Uani 1 1 d . . . . .
 H7A H 0.489604 0.280018 0.811184 0.026 Uiso 1 1 calc R U . . .
 H7B H 0.487040 0.366257 0.874187 0.026 Uiso 1 1 calc R U . . .
 H7C H 0.584560 0.291929 0.880510 0.026 Uiso 1 1 calc R U . . .
 C8 C 0.7216(2) 0.2193(2) 0.69602(15) 0.0171(5) Uani 1 1 d . . . . .
 H8 H 0.649021 0.181141 0.677184 0.021 Uiso 1 1 calc R U . . .
 C9 C 0.7681(2) 0.2122(2) 0.76685(15) 0.0192(6) Uani 1 1 d . . . . .
 H9 H 0.727498 0.168786 0.795114 0.023 Uiso 1 1 calc R U . . .
 C10 C 0.8746(2) 0.2693(2) 0.79595(16) 0.0206(6) Uani 1 1 d . . . . .
 H10 H 0.907018 0.263621 0.843532 0.025 Uiso 1 1 calc R U . . .
 C11 C 0.9324(2) 0.3347(2) 0.75405(15) 0.0195(6) Uani 1 1 d . . . . .
 H11 H 1.003543 0.374715 0.773633 0.023 Uiso 1 1 calc R U . . .
 C12 C 0.8857(2) 0.3413(2) 0.68337(15) 0.0165(5) Uani 1 1 d . . . . .
 H12 H 0.925696 0.386462 0.655838 0.020 Uiso 1 1 calc R U . . .
 C13 C 0.7805(2) 0.28219(19) 0.65207(14) 0.0152(5) Uani 1 1 d . . . . .
 C14 C 0.7341(2) 0.2853(2) 0.57586(15) 0.0189(6) Uani 1 1 d . . . . .
 H14A H 0.661469 0.313917 0.571574 0.028 Uiso 1 1 calc R U . . .
 H14B H 0.721519 0.214855 0.552199 0.028 Uiso 1 1 calc R U . . .
 H14C H 0.788971 0.329305 0.553739 0.028 Uiso 1 1 calc R U . . .
 Cl1 Cl 0.49325(5) 0.82086(5) 0.98657(3) 0.01953(14) Uani 1 1 d . . . . .
 Cl2 Cl 0.26637(6) 0.96226(5) 0.92129(3) 0.01822(14) Uani 1 1 d . . . . .
 Cl3 Cl 0.17872(6) 0.87607(5) 0.73776(3) 0.01809(14) Uani 1 1 d . . . . .
 Cl4 Cl 0.34324(6) 0.67863(5) 0.69140(3) 0.02082(14) Uani 1 1 d . . . . .
 Cl5 Cl 0.53951(5) 0.64732(5) 0.84636(4) 0.02284(15) Uani 1 1 d . . . . .
 Cl6 Cl 0.20115(5) 0.74390(5) 1.02822(3) 0.01818(14) Uani 1 1 d . . . . .
 Cl7 Cl -0.00232(5) 0.77504(5) 0.86878(3) 0.01575(13) Uani 1 1 d . . . . .
 Cl8 Cl 0.04664(5) 0.59584(5) 0.72554(3) 0.01439(13) Uani 1 1 d . . . . .
 Cl9 Cl 0.27855(6) 0.45272(5) 0.79252(3) 0.01912(14) Uani 1 1 d . . . . .
 Cl10 Cl 0.37464(6) 0.54182(5) 0.97934(3) 0.02069(14) Uani 1 1 d . . . . .
 Cl11 Cl 0.07093(5) 0.51700(5) 0.90769(3) 0.01691(13) Uani 1 1 d . . . . .
 C15 C 0.3572(2) 0.7914(2) 0.83788(13) 0.0132(5) Uani 1 1 d . . . . .
 H15 H 0.421624 0.852700 0.823029 0.016 Uiso 1 1 calc R U . . .
 B1 B 0.3760(3) 0.7600(2) 0.92385(16) 0.0140(6) Uani 1 1 d . . . . .
 B2 B 0.2634(2) 0.8307(2) 0.89059(15) 0.0128(6) Uani 1 1 d . . . . .
 B3 B 0.2167(3) 0.7872(2) 0.79855(15) 0.0124(6) Uani 1 1 d . . . . .
 B4 B 0.3011(3) 0.6887(2) 0.77569(15) 0.0134(6) Uani 1 1 d . . . . .
 B5 B 0.3989(3) 0.6726(2) 0.85292(16) 0.0154(6) Uani 1 1 d . . . . .
 B6 B 0.2355(2) 0.7245(2) 0.94127(15) 0.0123(6) Uani 1 1 d . . . . .
 B7 B 0.1363(2) 0.7408(2) 0.86399(14) 0.0105(5) Uani 1 1 d . . . . .
 B8 B 0.1600(2) 0.6526(2) 0.79335(15) 0.0116(5) Uani 1 1 d . . . . .
 B9 B 0.2734(2) 0.5819(2) 0.82663(15) 0.0126(6) Uani 1 1 d . . . . .
 B10 B 0.3199(2) 0.6261(2) 0.91833(15) 0.0128(6) Uani 1 1 d . . . . .
 B11 B 0.1715(2) 0.6144(2) 0.88150(15) 0.0121(6) Uani 1 1 d . . . . .
 Cl12 Cl 0.27156(5) 0.00582(5) 0.39852(3) 0.01685(13) Uani 1 1 d . . . . .
 Cl13 Cl 0.19879(5) -0.02242(5) 0.57101(3) 0.01692(13) Uani 1 1 d . . . . .
 Cl14 Cl -0.00336(5) 0.14797(5) 0.59855(3) 0.01568(13) Uani 1 1 d . . . . .
 Cl15 Cl -0.05611(5) 0.28591(5) 0.44359(3) 0.01625(13) Uani 1 1 d . . . . .
 Cl16 Cl 0.11767(5) 0.19446(5) 0.32002(3) 0.01663(13) Uani 1 1 d . . . . .
 Cl17 Cl 0.42158(5) 0.27561(5) 0.39643(3) 0.01860(14) Uani 1 1 d . . . . .
 Cl18 Cl 0.47204(5) 0.12866(5) 0.55486(4) 0.02129(14) Uani 1 1 d . . . . .
 Cl19 Cl 0.30004(6) 0.22710(5) 0.68226(3) 0.01976(14) Uani 1 1 d . . . . .
 Cl20 Cl 0.13802(6) 0.42281(5) 0.60091(3) 0.01754(13) Uani 1 1 d . . . . .
 Cl21 Cl 0.21049(6) 0.45093(5) 0.42575(3) 0.01655(13) Uani 1 1 d . . . . .
 Cl22 Cl 0.43246(5) 0.41106(5) 0.56964(3) 0.01915(14) Uani 1 1 d . . . . .
 C16 C 0.1117(2) 0.12927(18) 0.46853(13) 0.0100(5) Uani 1 1 d . . . . .
 H16 H 0.040050 0.066835 0.445438 0.012 Uiso 1 1 calc R U . . .
 B12 B 0.2466(2) 0.1149(2) 0.45108(15) 0.0118(5) Uani 1 1 d . . . . .
 B13 B 0.2094(2) 0.1004(2) 0.53738(15) 0.0125(6) Uani 1 1 d . . . . .
 B14 B 0.1085(2) 0.1875(2) 0.55097(15) 0.0113(5) Uani 1 1 d . . . . .
 B15 B 0.0811(2) 0.2550(2) 0.47359(15) 0.0108(5) Uani 1 1 d . . . . .
 B16 B 0.1678(2) 0.2100(2) 0.41170(15) 0.0125(6) Uani 1 1 d . . . . .
 B17 B 0.3146(2) 0.2443(2) 0.44970(15) 0.0120(5) Uani 1 1 d . . . . .
 B18 B 0.3403(3) 0.1759(2) 0.52725(16) 0.0139(6) Uani 1 1 d . . . . .
 B19 B 0.2550(3) 0.2213(2) 0.58953(15) 0.0131(6) Uani 1 1 d . . . . .
 B20 B 0.1748(3) 0.3168(2) 0.55006(15) 0.0120(6) Uani 1 1 d . . . . .
 B21 B 0.2116(2) 0.3298(2) 0.46350(15) 0.0108(5) Uani 1 1 d . . . . .
 B22 B 0.3192(2) 0.3100(2) 0.53513(15) 0.0122(6) Uani 1 1 d . . . . .
 C17 C 0.5829(3) 1.0122(2) 0.86804(17) 0.0308(7) Uani 1 1 d . . . . .
 H17 H 0.600709 1.033317 0.917182 0.037 Uiso 1 1 calc R U . . .
 C18 C 0.4963(3) 1.0518(2) 0.8261(2) 0.0340(8) Uani 1 1 d . . . . .
 H18 H 0.454504 1.099640 0.847165 0.041 Uiso 1 1 calc R U . . .
 C19 C 0.4699(3) 1.0233(3) 0.7549(2) 0.0363(8) Uani 1 1 d . . . . .
 H19 H 0.410542 1.051226 0.726790 0.044 Uiso 1 1 calc R U . . .
 C20 C 0.5298(3) 0.9543(3) 0.72494(18) 0.0345(8) Uani 1 1 d . . . . .
 H20 H 0.511457 0.934409 0.675657 0.041 Uiso 1 1 calc R U . . .
 C21 C 0.6159(3) 0.9131(3) 0.76437(19) 0.0334(8) Uani 1 1 d . . . . .
 H21 H 0.656866 0.865611 0.742302 0.040 Uiso 1 1 calc R U . . .
 C22 C 0.6437(3) 0.9413(3) 0.8376(2) 0.0323(7) Uani 1 1 d . . . . .
 C23 C 0.7324(3) 0.8935(3) 0.8832(3) 0.0514(11) Uani 1 1 d . . . . .
 H23A H 0.759763 0.938651 0.926913 0.077 Uiso 1 1 calc R U . . .
 H23B H 0.796630 0.885092 0.857909 0.077 Uiso 1 1 calc R U . . .
 H23C H 0.698888 0.825418 0.894710 0.077 Uiso 1 1 calc R U . . .
 C24 C 0.9473(4) 0.8563(4) 0.0607(3) 0.0376(6) Uani 0.795(6) 1 d D U P A 1
 H24 H 0.961765 0.851684 0.013391 0.045 Uiso 0.795(6) 1 calc R U P A 1
 C25 C 1.0128(5) 0.9286(4) 0.1092(3) 0.0402(7) Uani 0.795(6) 1 d D U P A 1
 H25 H 1.073001 0.973743 0.095579 0.048 Uiso 0.795(6) 1 calc R U P A 1
 C26 C 0.9927(5) 0.9371(4) 0.1785(3) 0.0416(7) Uani 0.795(6) 1 d D U P A 1
 H26 H 1.040016 0.986877 0.212366 0.050 Uiso 0.795(6) 1 calc R U P A 1
 C27 C 0.9051(5) 0.8741(4) 0.1980(3) 0.0408(7) Uani 0.795(6) 1 d D U P A 1
 H27 H 0.888864 0.881784 0.244841 0.049 Uiso 0.795(6) 1 calc R U P A 1
 C28 C 0.8415(4) 0.8007(4) 0.1504(3) 0.0402(7) Uani 0.795(6) 1 d D U P A 1
 H28 H 0.782632 0.755238 0.165134 0.048 Uiso 0.795(6) 1 calc R U P A 1
 C29 C 0.8594(5) 0.7892(4) 0.0797(3) 0.0400(6) Uani 0.795(6) 1 d D U P A 1
 C30 C 0.7784(4) 0.7136(3) 0.0298(3) 0.0468(11) Uani 0.795(6) 1 d D U P A 1
 H30A H 0.709401 0.744609 0.013889 0.070 Uiso 0.795(6) 1 calc R U P A 1
 H30B H 0.757708 0.651287 0.053469 0.070 Uiso 0.795(6) 1 calc R U P A 1
 H30C H 0.814379 0.694566 -0.010994 0.070 Uiso 0.795(6) 1 calc R U P A 1
 C24A C 0.8458(15) 0.7959(14) 0.0819(10) 0.0398(7) Uani 0.205(6) 1 d D U P A
 2
 H24A H 0.789146 0.748337 0.052043 0.048 Uiso 0.205(6) 1 calc R U P A 2
 C25A C 0.9428(15) 0.8351(13) 0.0580(10) 0.0390(7) Uani 0.205(6) 1 d D U P A
 2
 H25A H 0.954270 0.812647 0.011848 0.047 Uiso 0.205(6) 1 calc R U P A 2
 C26A C 1.0235(15) 0.9057(13) 0.0989(10) 0.0398(8) Uani 0.205(6) 1 d D U P A
 2
 H26A H 1.091061 0.930191 0.081046 0.048 Uiso 0.205(6) 1 calc R U P A 2
 C27A C 1.0100(16) 0.9425(15) 0.1654(10) 0.0405(8) Uani 0.205(6) 1 d D U P A
 2
 H27A H 1.062307 0.997423 0.191726 0.049 Uiso 0.205(6) 1 calc R U P A 2
 C28A C 0.9160(15) 0.8959(14) 0.1928(10) 0.0406(8) Uani 0.205(6) 1 d D U P A
 2
 H28A H 0.910524 0.912103 0.241072 0.049 Uiso 0.205(6) 1 calc R U P A 2
 C29A C 0.8302(13) 0.8263(13) 0.1510(9) 0.0399(7) Uani 0.205(6) 1 d D U P A 2
 C30A C 0.7111(12) 0.7796(12) 0.1586(9) 0.0346(16) Uani 0.205(6) 1 d D U P A
 2
 H30D H 0.694735 0.709015 0.135072 0.052 Uiso 0.205(6) 1 calc R U P A 2
 H30E H 0.655620 0.822152 0.136817 0.052 Uiso 0.205(6) 1 calc R U P A 2
 H30F H 0.705350 0.777336 0.208818 0.052 Uiso 0.205(6) 1 calc R U P A 2


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 Ni1 C1 2.263(3) . ?
 Ni1 C2 2.274(2) . ?
 Ni1 C3 2.276(3) . ?
 Ni1 C4 2.250(3) . ?
 Ni1 C5 2.243(3) . ?
 Ni1 C6 2.284(3) . ?
 Ni1 C8 2.256(3) . ?
 Ni1 C9 2.245(3) . ?
 Ni1 C10 2.261(3) . ?
 Ni1 C11 2.255(3) . ?
 Ni1 C12 2.270(3) . ?
 Ni1 C13 2.320(3) . ?
 C1 H1 0.9500 . ?
 C1 C2 1.399(4) . ?
 C1 C6 1.413(3) . ?
 C2 H2 0.9500 . ?
 C2 C3 1.407(4) . ?
 C3 H3 0.9500 . ?
 C3 C4 1.408(4) . ?
 C4 H4 0.9500 . ?
 C4 C5 1.402(4) . ?
 C5 H5 0.9500 . ?
 C5 C6 1.418(4) . ?
 C6 C7 1.491(4) . ?
 C7 H7A 0.9800 . ?
 C7 H7B 0.9800 . ?
 C7 H7C 0.9800 . ?
 C8 H8 0.9500 . ?
 C8 C9 1.405(4) . ?
 C8 C13 1.417(4) . ?
 C9 H9 0.9500 . ?
 C9 C10 1.406(4) . ?
 C10 H10 0.9500 . ?
 C10 C11 1.401(4) . ?
 C11 H11 0.9500 . ?
 C11 C12 1.402(4) . ?
 C12 H12 0.9500 . ?
 C12 C13 1.415(4) . ?
 C13 C14 1.492(4) . ?
 C14 H14A 0.9800 . ?
 C14 H14B 0.9800 . ?
 C14 H14C 0.9800 . ?
 Cl1 B1 1.769(3) . ?
 Cl2 B2 1.769(3) . ?
 Cl3 B3 1.753(3) . ?
 Cl4 B4 1.768(3) . ?
 Cl5 B5 1.770(3) . ?
 Cl6 B6 1.787(3) . ?
 Cl7 B7 1.779(3) . ?
 Cl8 B8 1.780(3) . ?
 Cl9 B9 1.775(3) . ?
 Cl10 B10 1.771(3) . ?
 Cl11 B11 1.787(3) . ?
 C15 H15 1.1200 . ?
 C15 B1 1.719(4) . ?
 C15 B2 1.717(4) . ?
 C15 B3 1.725(4) . ?
 C15 B4 1.728(4) . ?
 C15 B5 1.715(4) . ?
 B1 B2 1.788(4) . ?
 B1 B5 1.790(4) . ?
 B1 B6 1.770(4) . ?
 B1 B10 1.779(4) . ?
 B2 B3 1.802(4) . ?
 B2 B6 1.772(4) . ?
 B2 B7 1.782(4) . ?
 B3 B4 1.796(4) . ?
 B3 B7 1.786(4) . ?
 B3 B8 1.789(4) . ?
 B4 B5 1.789(4) . ?
 B4 B8 1.778(4) . ?
 B4 B9 1.782(4) . ?
 B5 B9 1.774(4) . ?
 B5 B10 1.775(4) . ?
 B6 B7 1.799(4) . ?
 B6 B10 1.797(4) . ?
 B6 B11 1.788(4) . ?
 B7 B8 1.796(4) . ?
 B7 B11 1.792(4) . ?
 B8 B9 1.795(4) . ?
 B8 B11 1.789(4) . ?
 B9 B10 1.798(4) . ?
 B9 B11 1.794(4) . ?
 B10 B11 1.790(4) . ?
 Cl12 B12 1.768(3) . ?
 Cl13 B13 1.764(3) . ?
 Cl14 B14 1.772(3) . ?
 Cl15 B15 1.758(3) . ?
 Cl16 B16 1.763(3) . ?
 Cl17 B17 1.778(3) . ?
 Cl18 B18 1.780(3) . ?
 Cl19 B19 1.777(3) . ?
 Cl20 B20 1.774(3) . ?
 Cl21 B21 1.783(3) . ?
 Cl22 B22 1.780(3) . ?
 C16 H16 1.1200 . ?
 C16 B12 1.721(4) . ?
 C16 B13 1.723(4) . ?
 C16 B14 1.717(4) . ?
 C16 B15 1.722(4) . ?
 C16 B16 1.717(4) . ?
 B12 B13 1.795(4) . ?
 B12 B16 1.789(4) . ?
 B12 B17 1.782(4) . ?
 B12 B18 1.777(4) . ?
 B13 B14 1.789(4) . ?
 B13 B18 1.783(4) . ?
 B13 B19 1.785(4) . ?
 B14 B15 1.788(4) . ?
 B14 B19 1.782(4) . ?
 B14 B20 1.773(4) . ?
 B15 B16 1.803(4) . ?
 B15 B20 1.784(4) . ?
 B15 B21 1.776(4) . ?
 B16 B17 1.783(4) . ?
 B16 B21 1.769(4) . ?
 B17 B18 1.797(4) . ?
 B17 B21 1.793(4) . ?
 B17 B22 1.788(4) . ?
 B18 B19 1.798(4) . ?
 B18 B22 1.797(4) . ?
 B19 B20 1.803(4) . ?
 B19 B22 1.789(4) . ?
 B20 B21 1.796(4) . ?
 B20 B22 1.800(4) . ?
 B21 B22 1.793(4) . ?
 C17 H17 0.9500 . ?
 C17 C18 1.388(5) . ?
 C17 C22 1.393(5) . ?
 C18 H18 0.9500 . ?
 C18 C19 1.373(5) . ?
 C19 H19 0.9500 . ?
 C19 C20 1.364(5) . ?
 C20 H20 0.9500 . ?
 C20 C21 1.371(5) . ?
 C21 H21 0.9500 . ?
 C21 C22 1.408(5) . ?
 C22 C23 1.497(5) . ?
 C23 H23A 0.9800 . ?
 C23 H23B 0.9800 . ?
 C23 H23C 0.9800 . ?
 C24 H24 0.9500 . ?
 C24 C25 1.359(6) . ?
 C24 C29 1.389(6) . ?
 C25 H25 0.9500 . ?
 C25 C26 1.388(6) . ?
 C26 H26 0.9500 . ?
 C26 C27 1.361(6) . ?
 C27 H27 0.9500 . ?
 C27 C28 1.349(6) . ?
 C28 H28 0.9500 . ?
 C28 C29 1.408(6) . ?
 C29 C30 1.477(7) . ?
 C30 H30A 0.9800 . ?
 C30 H30B 0.9800 . ?
 C30 H30C 0.9800 . ?
 C24A H24A 0.9500 . ?
 C24A C25A 1.361(11) . ?
 C24A C29A 1.405(11) . ?
 C25A H25A 0.9500 . ?
 C25A C26A 1.358(11) . ?
 C26A H26A 0.9500 . ?
 C26A C27A 1.373(11) . ?
 C27A H27A 0.9500 . ?
 C27A C28A 1.398(11) . ?
 C28A H28A 0.9500 . ?
 C28A C29A 1.393(11) . ?
 C29A C30A 1.507(14) . ?
 C30A H30D 0.9800 . ?
 C30A H30E 0.9800 . ?
 C30A H30F 0.9800 . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 C1 Ni1 C2 35.91(9) . . ?
 C1 Ni1 C3 64.75(9) . . ?
 C1 Ni1 C6 36.21(9) . . ?
 C1 Ni1 C12 140.42(10) . . ?
 C1 Ni1 C13 112.37(9) . . ?
 C2 Ni1 C3 36.02(9) . . ?
 C2 Ni1 C6 65.20(9) . . ?
 C2 Ni1 C13 105.12(9) . . ?
 C3 Ni1 C6 77.25(9) . . ?
 C3 Ni1 C13 120.27(9) . . ?
 C4 Ni1 C1 76.52(9) . . ?
 C4 Ni1 C2 64.91(9) . . ?
 C4 Ni1 C3 36.25(9) . . ?
 C4 Ni1 C6 65.54(9) . . ?
 C4 Ni1 C8 173.00(10) . . ?
 C4 Ni1 C10 111.56(10) . . ?
 C4 Ni1 C11 104.59(10) . . ?
 C4 Ni1 C12 120.47(10) . . ?
 C4 Ni1 C13 150.73(10) . . ?
 C5 Ni1 C1 65.02(9) . . ?
 C5 Ni1 C2 76.79(9) . . ?
 C5 Ni1 C3 65.35(9) . . ?
 C5 Ni1 C4 36.36(10) . . ?
 C5 Ni1 C6 36.51(9) . . ?
 C5 Ni1 C8 136.94(10) . . ?
 C5 Ni1 C9 109.37(10) . . ?
 C5 Ni1 C10 101.61(10) . . ?
 C5 Ni1 C11 117.91(10) . . ?
 C5 Ni1 C12 149.67(10) . . ?
 C5 Ni1 C13 172.82(10) . . ?
 C6 Ni1 C13 137.79(10) . . ?
 C8 Ni1 C1 102.69(10) . . ?
 C8 Ni1 C2 118.48(10) . . ?
 C8 Ni1 C3 149.62(10) . . ?
 C8 Ni1 C6 109.64(10) . . ?
 C8 Ni1 C10 65.27(10) . . ?
 C8 Ni1 C12 64.56(10) . . ?
 C8 Ni1 C13 36.04(9) . . ?
 C9 Ni1 C1 116.39(10) . . ?
 C9 Ni1 C2 147.69(10) . . ?
 C9 Ni1 C3 173.96(10) . . ?
 C9 Ni1 C4 137.71(10) . . ?
 C9 Ni1 C6 100.26(10) . . ?
 C9 Ni1 C8 36.39(10) . . ?
 C9 Ni1 C10 36.37(11) . . ?
 C9 Ni1 C11 65.16(10) . . ?
 C9 Ni1 C12 76.60(10) . . ?
 C9 Ni1 C13 65.25(10) . . ?
 C10 Ni1 C1 146.75(10) . . ?
 C10 Ni1 C2 175.91(10) . . ?
 C10 Ni1 C3 139.89(10) . . ?
 C10 Ni1 C6 115.74(10) . . ?
 C10 Ni1 C12 64.93(10) . . ?
 C10 Ni1 C13 76.94(10) . . ?
 C11 Ni1 C1 176.41(10) . . ?
 C11 Ni1 C2 141.39(10) . . ?
 C11 Ni1 C3 114.09(10) . . ?
 C11 Ni1 C6 147.37(10) . . ?
 C11 Ni1 C8 76.64(10) . . ?
 C11 Ni1 C10 36.16(10) . . ?
 C11 Ni1 C12 36.09(10) . . ?
 C11 Ni1 C13 64.99(10) . . ?
 C12 Ni1 C2 114.63(10) . . ?
 C12 Ni1 C3 106.41(10) . . ?
 C12 Ni1 C6 173.67(10) . . ?
 C12 Ni1 C13 35.90(10) . . ?
 Ni1 C1 H1 127.9 . . ?
 C2 C1 Ni1 72.45(15) . . ?
 C2 C1 H1 119.2 . . ?
 C2 C1 C6 121.7(2) . . ?
 C6 C1 Ni1 72.68(14) . . ?
 C6 C1 H1 119.2 . . ?
 Ni1 C2 H2 128.6 . . ?
 C1 C2 Ni1 71.64(14) . . ?
 C1 C2 H2 119.9 . . ?
 C1 C2 C3 120.1(2) . . ?
 C3 C2 Ni1 72.07(14) . . ?
 C3 C2 H2 119.9 . . ?
 Ni1 C3 H3 129.1 . . ?
 C2 C3 Ni1 71.91(14) . . ?
 C2 C3 H3 120.4 . . ?
 C2 C3 C4 119.2(2) . . ?
 C4 C3 Ni1 70.88(15) . . ?
 C4 C3 H3 120.4 . . ?
 Ni1 C4 H4 128.0 . . ?
 C3 C4 Ni1 72.87(15) . . ?
 C3 C4 H4 119.8 . . ?
 C5 C4 Ni1 71.54(15) . . ?
 C5 C4 C3 120.5(2) . . ?
 C5 C4 H4 119.8 . . ?
 Ni1 C5 H5 127.1 . . ?
 C4 C5 Ni1 72.10(15) . . ?
 C4 C5 H5 119.5 . . ?
 C4 C5 C6 121.0(2) . . ?
 C6 C5 Ni1 73.31(15) . . ?
 C6 C5 H5 119.5 . . ?
 C1 C6 Ni1 71.11(14) . . ?
 C1 C6 C5 117.6(2) . . ?
 C1 C6 C7 120.8(2) . . ?
 C5 C6 Ni1 70.18(14) . . ?
 C5 C6 C7 121.6(2) . . ?
 C7 C6 Ni1 129.77(18) . . ?
 C6 C7 H7A 109.5 . . ?
 C6 C7 H7B 109.5 . . ?
 C6 C7 H7C 109.5 . . ?
 H7A C7 H7B 109.5 . . ?
 H7A C7 H7C 109.5 . . ?
 H7B C7 H7C 109.5 . . ?
 Ni1 C8 H8 127.0 . . ?
 C9 C8 Ni1 71.36(15) . . ?
 C9 C8 H8 119.3 . . ?
 C9 C8 C13 121.4(3) . . ?
 C13 C8 Ni1 74.42(15) . . ?
 C13 C8 H8 119.3 . . ?
 Ni1 C9 H9 127.4 . . ?
 C8 C9 Ni1 72.26(15) . . ?
 C8 C9 H9 119.9 . . ?
 C8 C9 C10 120.1(3) . . ?
 C10 C9 Ni1 72.44(15) . . ?
 C10 C9 H9 119.9 . . ?
 Ni1 C10 H10 129.0 . . ?
 C9 C10 Ni1 71.20(15) . . ?
 C9 C10 H10 120.3 . . ?
 C11 C10 Ni1 71.71(16) . . ?
 C11 C10 C9 119.3(3) . . ?
 C11 C10 H10 120.3 . . ?
 Ni1 C11 H11 127.6 . . ?
 C10 C11 Ni1 72.14(16) . . ?
 C10 C11 H11 119.8 . . ?
 C10 C11 C12 120.3(3) . . ?
 C12 C11 Ni1 72.52(15) . . ?
 C12 C11 H11 119.8 . . ?
 Ni1 C12 H12 127.6 . . ?
 C11 C12 Ni1 71.39(16) . . ?
 C11 C12 H12 119.2 . . ?
 C11 C12 C13 121.5(3) . . ?
 C13 C12 Ni1 73.97(15) . . ?
 C13 C12 H12 119.2 . . ?
 C8 C13 Ni1 69.54(15) . . ?
 C8 C13 C14 121.5(2) . . ?
 C12 C13 Ni1 70.13(15) . . ?
 C12 C13 C8 117.2(2) . . ?
 C12 C13 C14 121.3(2) . . ?
 C14 C13 Ni1 131.89(18) . . ?
 C13 C14 H14A 109.5 . . ?
 C13 C14 H14B 109.5 . . ?
 C13 C14 H14C 109.5 . . ?
 H14A C14 H14B 109.5 . . ?
 H14A C14 H14C 109.5 . . ?
 H14B C14 H14C 109.5 . . ?
 B1 C15 H15 117.5 . . ?
 B1 C15 B3 115.2(2) . . ?
 B1 C15 B4 114.9(2) . . ?
 B2 C15 H15 117.5 . . ?
 B2 C15 B1 62.71(16) . . ?
 B2 C15 B3 63.15(16) . . ?
 B2 C15 B4 114.9(2) . . ?
 B3 C15 H15 117.4 . . ?
 B3 C15 B4 62.68(16) . . ?
 B4 C15 H15 117.7 . . ?
 B5 C15 H15 117.8 . . ?
 B5 C15 B1 62.84(16) . . ?
 B5 C15 B2 114.7(2) . . ?
 B5 C15 B3 114.7(2) . . ?
 B5 C15 B4 62.61(17) . . ?
 Cl1 B1 B2 120.72(19) . . ?
 Cl1 B1 B5 120.10(19) . . ?
 Cl1 B1 B6 125.4(2) . . ?
 Cl1 B1 B10 124.55(19) . . ?
 C15 B1 Cl1 121.5(2) . . ?
 C15 B1 B2 58.60(15) . . ?
 C15 B1 B5 58.49(16) . . ?
 C15 B1 B6 104.4(2) . . ?
 C15 B1 B10 104.5(2) . . ?
 B2 B1 B5 107.8(2) . . ?
 B6 B1 B2 59.76(16) . . ?
 B6 B1 B5 108.0(2) . . ?
 B6 B1 B10 60.83(16) . . ?
 B10 B1 B2 108.5(2) . . ?
 B10 B1 B5 59.65(17) . . ?
 Cl2 B2 B1 120.31(19) . . ?
 Cl2 B2 B3 120.60(18) . . ?
 Cl2 B2 B6 124.32(19) . . ?
 Cl2 B2 B7 124.61(19) . . ?
 C15 B2 Cl2 122.29(19) . . ?
 C15 B2 B1 58.68(15) . . ?
 C15 B2 B3 58.64(15) . . ?
 C15 B2 B6 104.37(19) . . ?
 C15 B2 B7 104.35(19) . . ?
 B1 B2 B3 108.2(2) . . ?
 B6 B2 B1 59.62(16) . . ?
 B6 B2 B3 108.4(2) . . ?
 B6 B2 B7 60.80(16) . . ?
 B7 B2 B1 108.3(2) . . ?
 B7 B2 B3 59.75(16) . . ?
 Cl3 B3 B2 120.22(18) . . ?
 Cl3 B3 B4 119.90(19) . . ?
 Cl3 B3 B7 126.47(19) . . ?
 Cl3 B3 B8 126.51(19) . . ?
 C15 B3 Cl3 120.42(19) . . ?
 C15 B3 B2 58.21(15) . . ?
 C15 B3 B4 58.73(16) . . ?
 C15 B3 B7 103.87(19) . . ?
 C15 B3 B8 103.94(19) . . ?
 B4 B3 B2 107.6(2) . . ?
 B7 B3 B2 59.56(16) . . ?
 B7 B3 B4 107.8(2) . . ?
 B7 B3 B8 60.30(16) . . ?
 B8 B3 B2 107.6(2) . . ?
 B8 B3 B4 59.48(16) . . ?
 Cl4 B4 B3 120.51(19) . . ?
 Cl4 B4 B5 120.31(19) . . ?
 Cl4 B4 B8 125.23(19) . . ?
 Cl4 B4 B9 124.55(19) . . ?
 C15 B4 Cl4 121.94(19) . . ?
 C15 B4 B3 58.59(15) . . ?
 C15 B4 B5 58.36(16) . . ?
 C15 B4 B8 104.29(19) . . ?
 C15 B4 B9 104.2(2) . . ?
 B5 B4 B3 107.9(2) . . ?
 B8 B4 B3 60.08(16) . . ?
 B8 B4 B5 107.8(2) . . ?
 B8 B4 B9 60.55(16) . . ?
 B9 B4 B3 108.6(2) . . ?
 B9 B4 B5 59.57(16) . . ?
 Cl5 B5 B1 119.48(19) . . ?
 Cl5 B5 B4 120.7(2) . . ?
 Cl5 B5 B9 124.96(19) . . ?
 Cl5 B5 B10 124.1(2) . . ?
 C15 B5 Cl5 121.4(2) . . ?
 C15 B5 B1 58.67(16) . . ?
 C15 B5 B4 59.04(16) . . ?
 C15 B5 B9 105.1(2) . . ?
 C15 B5 B10 104.9(2) . . ?
 B4 B5 B1 108.5(2) . . ?
 B9 B5 B1 108.7(2) . . ?
 B9 B5 B4 60.03(16) . . ?
 B9 B5 B10 60.89(17) . . ?
 B10 B5 B1 59.87(17) . . ?
 B10 B5 B4 108.8(2) . . ?
 Cl6 B6 B7 121.70(18) . . ?
 Cl6 B6 B10 121.79(18) . . ?
 Cl6 B6 B11 122.40(19) . . ?
 B1 B6 Cl6 121.29(19) . . ?
 B1 B6 B2 60.62(16) . . ?
 B1 B6 B7 108.3(2) . . ?
 B1 B6 B10 59.84(16) . . ?
 B1 B6 B11 107.7(2) . . ?
 B2 B6 Cl6 121.15(19) . . ?
 B2 B6 B7 59.87(16) . . ?
 B2 B6 B10 108.4(2) . . ?
 B2 B6 B11 107.8(2) . . ?
 B10 B6 B7 108.2(2) . . ?
 B11 B6 B7 59.93(15) . . ?
 B11 B6 B10 59.92(16) . . ?
 Cl7 B7 B2 122.44(18) . . ?
 Cl7 B7 B3 121.33(18) . . ?
 Cl7 B7 B6 122.52(18) . . ?
 Cl7 B7 B8 121.04(18) . . ?
 Cl7 B7 B11 121.88(19) . . ?
 B2 B7 B3 60.69(16) . . ?
 B2 B7 B6 59.33(16) . . ?
 B2 B7 B8 108.2(2) . . ?
 B2 B7 B11 107.23(19) . . ?
 B3 B7 B6 108.0(2) . . ?
 B3 B7 B8 59.95(16) . . ?
 B3 B7 B11 107.8(2) . . ?
 B8 B7 B6 107.74(19) . . ?
 B11 B7 B6 59.74(16) . . ?
 B11 B7 B8 59.83(15) . . ?
 Cl8 B8 B3 121.66(18) . . ?
 Cl8 B8 B7 121.65(18) . . ?
 Cl8 B8 B9 121.52(19) . . ?
 Cl8 B8 B11 121.95(19) . . ?
 B3 B8 B7 59.75(16) . . ?
 B3 B8 B9 108.3(2) . . ?
 B4 B8 Cl8 121.75(19) . . ?
 B4 B8 B3 60.44(16) . . ?
 B4 B8 B7 108.1(2) . . ?
 B4 B8 B9 59.83(16) . . ?
 B4 B8 B11 107.7(2) . . ?
 B9 B8 B7 108.28(19) . . ?
 B11 B8 B3 107.7(2) . . ?
 B11 B8 B7 59.97(15) . . ?
 B11 B8 B9 60.06(16) . . ?
 Cl9 B9 B4 121.06(19) . . ?
 Cl9 B9 B8 121.48(19) . . ?
 Cl9 B9 B10 122.38(18) . . ?
 Cl9 B9 B11 122.78(19) . . ?
 B4 B9 B8 59.62(16) . . ?
 B4 B9 B10 108.1(2) . . ?
 B4 B9 B11 107.32(19) . . ?
 B5 B9 Cl9 122.01(19) . . ?
 B5 B9 B4 60.40(17) . . ?
 B5 B9 B8 107.7(2) . . ?
 B5 B9 B10 59.59(17) . . ?
 B5 B9 B11 107.0(2) . . ?
 B8 B9 B10 107.9(2) . . ?
 B11 B9 B8 59.80(15) . . ?
 B11 B9 B10 59.79(16) . . ?
 Cl10 B10 B1 121.92(19) . . ?
 Cl10 B10 B5 121.24(19) . . ?
 Cl10 B10 B6 122.90(19) . . ?
 Cl10 B10 B9 121.08(18) . . ?
 Cl10 B10 B11 122.69(19) . . ?
 B1 B10 B6 59.33(16) . . ?
 B1 B10 B9 108.1(2) . . ?
 B1 B10 B11 107.2(2) . . ?
 B5 B10 B1 60.48(16) . . ?
 B5 B10 B6 107.5(2) . . ?
 B5 B10 B9 59.52(16) . . ?
 B5 B10 B11 107.1(2) . . ?
 B6 B10 B9 107.91(19) . . ?
 B11 B10 B6 59.80(16) . . ?
 B11 B10 B9 59.97(16) . . ?
 Cl11 B11 B6 120.56(19) . . ?
 Cl11 B11 B7 121.89(19) . . ?
 Cl11 B11 B8 122.67(19) . . ?
 Cl11 B11 B9 121.60(19) . . ?
 Cl11 B11 B10 120.19(18) . . ?
 B6 B11 B7 60.33(16) . . ?
 B6 B11 B8 108.5(2) . . ?
 B6 B11 B9 108.5(2) . . ?
 B6 B11 B10 60.28(16) . . ?
 B7 B11 B9 108.5(2) . . ?
 B8 B11 B7 60.19(15) . . ?
 B8 B11 B9 60.14(16) . . ?
 B8 B11 B10 108.5(2) . . ?
 B10 B11 B7 108.8(2) . . ?
 B10 B11 B9 60.24(16) . . ?
 B12 C16 H16 117.6 . . ?
 B12 C16 B13 62.83(16) . . ?
 B12 C16 B15 115.29(19) . . ?
 B13 C16 H16 117.5 . . ?
 B14 C16 H16 117.9 . . ?
 B14 C16 B12 114.64(19) . . ?
 B14 C16 B13 62.67(16) . . ?
 B14 C16 B15 62.67(15) . . ?
 B14 C16 B16 114.82(19) . . ?
 B15 C16 H16 117.2 . . ?
 B15 C16 B13 115.13(19) . . ?
 B16 C16 H16 117.5 . . ?
 B16 C16 B12 62.70(16) . . ?
 B16 C16 B13 114.96(19) . . ?
 B16 C16 B15 63.23(16) . . ?
 Cl12 B12 B13 120.29(18) . . ?
 Cl12 B12 B16 120.08(19) . . ?
 Cl12 B12 B17 125.05(19) . . ?
 Cl12 B12 B18 125.04(19) . . ?
 C16 B12 Cl12 121.43(18) . . ?
 C16 B12 B13 58.64(15) . . ?
 C16 B12 B16 58.54(15) . . ?
 C16 B12 B17 104.44(19) . . ?
 C16 B12 B18 104.6(2) . . ?
 B16 B12 B13 108.1(2) . . ?
 B17 B12 B13 108.3(2) . . ?
 B17 B12 B16 59.91(16) . . ?
 B18 B12 B13 59.87(16) . . ?
 B18 B12 B16 108.5(2) . . ?
 B18 B12 B17 60.64(16) . . ?
 Cl13 B13 B12 120.43(19) . . ?
 Cl13 B13 B14 120.84(18) . . ?
 Cl13 B13 B18 124.70(19) . . ?
 Cl13 B13 B19 124.90(19) . . ?
 C16 B13 Cl13 121.99(18) . . ?
 C16 B13 B12 58.53(15) . . ?
 C16 B13 B14 58.49(15) . . ?
 C16 B13 B18 104.24(19) . . ?
 C16 B13 B19 104.42(19) . . ?
 B14 B13 B12 107.67(19) . . ?
 B18 B13 B12 59.54(16) . . ?
 B18 B13 B14 108.0(2) . . ?
 B18 B13 B19 60.54(17) . . ?
 B19 B13 B12 107.97(19) . . ?
 B19 B13 B14 59.82(16) . . ?
 Cl14 B14 B13 118.76(18) . . ?
 Cl14 B14 B15 120.57(19) . . ?
 Cl14 B14 B19 124.50(18) . . ?
 Cl14 B14 B20 125.62(19) . . ?
 C16 B14 Cl14 120.87(18) . . ?
 C16 B14 B13 58.84(15) . . ?
 C16 B14 B15 58.80(15) . . ?
 C16 B14 B19 104.8(2) . . ?
 C16 B14 B20 104.92(19) . . ?
 B15 B14 B13 108.7(2) . . ?
 B19 B14 B13 59.99(16) . . ?
 B19 B14 B15 109.0(2) . . ?
 B20 B14 B13 109.0(2) . . ?
 B20 B14 B15 60.13(15) . . ?
 B20 B14 B19 60.94(16) . . ?
 Cl15 B15 B14 121.18(19) . . ?
 Cl15 B15 B16 120.46(18) . . ?
 Cl15 B15 B20 125.05(19) . . ?
 Cl15 B15 B21 125.10(18) . . ?
 C16 B15 Cl15 122.11(18) . . ?
 C16 B15 B14 58.52(15) . . ?
 C16 B15 B16 58.25(15) . . ?
 C16 B15 B20 104.22(19) . . ?
 C16 B15 B21 103.58(19) . . ?
 B14 B15 B16 107.35(19) . . ?
 B20 B15 B14 59.50(15) . . ?
 B20 B15 B16 107.9(2) . . ?
 B21 B15 B14 107.5(2) . . ?
 B21 B15 B16 59.25(16) . . ?
 B21 B15 B20 60.61(16) . . ?
 Cl16 B16 B12 119.21(19) . . ?
 Cl16 B16 B15 121.38(19) . . ?
 Cl16 B16 B17 124.00(19) . . ?
 Cl16 B16 B21 125.78(19) . . ?
 C16 B16 Cl16 121.84(18) . . ?
 C16 B16 B12 58.77(15) . . ?
 C16 B16 B15 58.52(15) . . ?
 C16 B16 B17 104.59(19) . . ?
 C16 B16 B21 104.07(19) . . ?
 B12 B16 B15 108.17(19) . . ?
 B17 B16 B12 59.87(16) . . ?
 B17 B16 B15 108.4(2) . . ?
 B21 B16 B12 108.2(2) . . ?
 B21 B16 B15 59.62(16) . . ?
 B21 B16 B17 60.63(16) . . ?
 Cl17 B17 B12 122.23(19) . . ?
 Cl17 B17 B16 121.36(19) . . ?
 Cl17 B17 B18 122.41(19) . . ?
 Cl17 B17 B21 121.51(18) . . ?
 Cl17 B17 B22 122.09(19) . . ?
 B12 B17 B16 60.22(16) . . ?
 B12 B17 B18 59.52(16) . . ?
 B12 B17 B21 107.4(2) . . ?
 B12 B17 B22 107.52(19) . . ?
 B16 B17 B18 107.8(2) . . ?
 B16 B17 B21 59.30(16) . . ?
 B16 B17 B22 107.5(2) . . ?
 B21 B17 B18 108.0(2) . . ?
 B22 B17 B18 60.15(16) . . ?
 B22 B17 B21 60.07(16) . . ?
 Cl18 B18 B13 119.29(18) . . ?
 Cl18 B18 B17 123.04(19) . . ?
 Cl18 B18 B19 121.95(19) . . ?
 Cl18 B18 B22 124.80(19) . . ?
 B12 B18 Cl18 120.0(2) . . ?
 B12 B18 B13 60.59(16) . . ?
 B12 B18 B17 59.84(16) . . ?
 B12 B18 B19 108.2(2) . . ?
 B12 B18 B22 107.4(2) . . ?
 B13 B18 B17 108.2(2) . . ?
 B13 B18 B19 59.81(16) . . ?
 B13 B18 B22 107.4(2) . . ?
 B17 B18 B19 107.9(2) . . ?
 B17 B18 B22 59.69(16) . . ?
 B22 B18 B19 59.70(16) . . ?
 Cl19 B19 B13 121.62(18) . . ?
 Cl19 B19 B14 121.76(19) . . ?
 Cl19 B19 B18 122.04(19) . . ?
 Cl19 B19 B20 121.66(19) . . ?
 Cl19 B19 B22 122.43(19) . . ?
 B13 B19 B18 59.66(16) . . ?
 B13 B19 B20 107.8(2) . . ?
 B13 B19 B22 107.6(2) . . ?
 B14 B19 B13 60.19(16) . . ?
 B14 B19 B18 107.6(2) . . ?
 B14 B19 B20 59.26(16) . . ?
 B14 B19 B22 107.14(19) . . ?
 B18 B19 B20 108.23(19) . . ?
 B22 B19 B18 60.10(16) . . ?
 B22 B19 B20 60.12(16) . . ?
 Cl20 B20 B15 121.38(19) . . ?
 Cl20 B20 B19 122.27(18) . . ?
 Cl20 B20 B21 121.75(18) . . ?
 Cl20 B20 B22 122.08(18) . . ?
 B14 B20 Cl20 122.49(19) . . ?
 B14 B20 B15 60.37(15) . . ?
 B14 B20 B19 59.79(16) . . ?
 B14 B20 B21 107.25(19) . . ?
 B14 B20 B22 107.1(2) . . ?
 B15 B20 B19 108.26(19) . . ?
 B15 B20 B21 59.47(15) . . ?
 B15 B20 B22 107.6(2) . . ?
 B21 B20 B19 107.4(2) . . ?
 B21 B20 B22 59.80(16) . . ?
 B22 B20 B19 59.57(16) . . ?
 Cl21 B21 B17 122.56(18) . . ?
 Cl21 B21 B20 120.30(18) . . ?
 Cl21 B21 B22 122.07(18) . . ?
 B15 B21 Cl21 120.18(18) . . ?
 B15 B21 B17 109.17(19) . . ?
 B15 B21 B20 59.92(16) . . ?
 B15 B21 B22 108.25(19) . . ?
 B16 B21 Cl21 121.83(18) . . ?
 B16 B21 B15 61.14(16) . . ?
 B16 B21 B17 60.08(16) . . ?
 B16 B21 B20 108.84(19) . . ?
 B16 B21 B22 107.98(19) . . ?
 B17 B21 B20 108.53(19) . . ?
 B22 B21 B17 59.84(16) . . ?
 B22 B21 B20 60.19(16) . . ?
 Cl22 B22 B17 120.44(19) . . ?
 Cl22 B22 B18 122.30(19) . . ?
 Cl22 B22 B19 122.71(19) . . ?
 Cl22 B22 B20 121.46(19) . . ?
 Cl22 B22 B21 120.59(18) . . ?
 B17 B22 B18 60.15(16) . . ?
 B17 B22 B19 108.62(19) . . ?
 B17 B22 B20 108.6(2) . . ?
 B17 B22 B21 60.09(16) . . ?
 B18 B22 B20 108.45(19) . . ?
 B19 B22 B18 60.20(16) . . ?
 B19 B22 B20 60.31(16) . . ?
 B19 B22 B21 108.2(2) . . ?
 B21 B22 B18 108.0(2) . . ?
 B21 B22 B20 60.01(16) . . ?
 C18 C17 H17 120.2 . . ?
 C18 C17 C22 119.6(3) . . ?
 C22 C17 H17 120.2 . . ?
 C17 C18 H18 119.4 . . ?
 C19 C18 C17 121.3(3) . . ?
 C19 C18 H18 119.4 . . ?
 C18 C19 H19 120.4 . . ?
 C20 C19 C18 119.2(3) . . ?
 C20 C19 H19 120.4 . . ?
 C19 C20 H20 119.3 . . ?
 C19 C20 C21 121.5(3) . . ?
 C21 C20 H20 119.3 . . ?
 C20 C21 H21 120.0 . . ?
 C20 C21 C22 120.0(3) . . ?
 C22 C21 H21 120.0 . . ?
 C17 C22 C21 118.5(3) . . ?
 C17 C22 C23 119.8(4) . . ?
 C21 C22 C23 121.7(4) . . ?
 C22 C23 H23A 109.5 . . ?
 C22 C23 H23B 109.5 . . ?
 C22 C23 H23C 109.5 . . ?
 H23A C23 H23B 109.5 . . ?
 H23A C23 H23C 109.5 . . ?
 H23B C23 H23C 109.5 . . ?
 C25 C24 H24 119.7 . . ?
 C25 C24 C29 120.6(5) . . ?
 C29 C24 H24 119.7 . . ?
 C24 C25 H25 119.7 . . ?
 C24 C25 C26 120.6(5) . . ?
 C26 C25 H25 119.7 . . ?
 C25 C26 H26 120.1 . . ?
 C27 C26 C25 119.9(5) . . ?
 C27 C26 H26 120.1 . . ?
 C26 C27 H27 120.2 . . ?
 C28 C27 C26 119.7(5) . . ?
 C28 C27 H27 120.2 . . ?
 C27 C28 H28 118.9 . . ?
 C27 C28 C29 122.2(5) . . ?
 C29 C28 H28 118.9 . . ?
 C24 C29 C28 117.0(5) . . ?
 C24 C29 C30 124.5(5) . . ?
 C28 C29 C30 118.3(5) . . ?
 C29 C30 H30A 109.5 . . ?
 C29 C30 H30B 109.5 . . ?
 C29 C30 H30C 109.5 . . ?
 H30A C30 H30B 109.5 . . ?
 H30A C30 H30C 109.5 . . ?
 H30B C30 H30C 109.5 . . ?
 C25A C24A H24A 120.2 . . ?
 C25A C24A C29A 119.6(14) . . ?
 C29A C24A H24A 120.2 . . ?
 C24A C25A H25A 119.3 . . ?
 C26A C25A C24A 121.4(14) . . ?
 C26A C25A H25A 119.3 . . ?
 C25A C26A H26A 119.2 . . ?
 C25A C26A C27A 121.6(13) . . ?
 C27A C26A H26A 119.2 . . ?
 C26A C27A H27A 121.3 . . ?
 C26A C27A C28A 117.3(13) . . ?
 C28A C27A H27A 121.3 . . ?
 C27A C28A H28A 119.3 . . ?
 C29A C28A C27A 121.5(13) . . ?
 C29A C28A H28A 119.3 . . ?
 C24A C29A C30A 106.8(12) . . ?
 C28A C29A C24A 118.1(12) . . ?
 C28A C29A C30A 134.8(13) . . ?
 C29A C30A H30D 109.5 . . ?
 C29A C30A H30E 109.5 . . ?
 C29A C30A H30F 109.5 . . ?
 H30D C30A H30E 109.5 . . ?
 H30D C30A H30F 109.5 . . ?
 H30E C30A H30F 109.5 . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 Ni1 C1 C2 C3 -55.4(2) . . . . ?
 Ni1 C1 C6 C5 54.3(2) . . . . ?
 Ni1 C1 C6 C7 -125.7(2) . . . . ?
 Ni1 C2 C3 C4 -54.8(2) . . . . ?
 Ni1 C3 C4 C5 -55.5(2) . . . . ?
 Ni1 C4 C5 C6 -56.9(2) . . . . ?
 Ni1 C5 C6 C1 -54.8(2) . . . . ?
 Ni1 C5 C6 C7 125.2(2) . . . . ?
 Ni1 C8 C9 C10 -56.5(2) . . . . ?
 Ni1 C8 C13 C12 53.2(2) . . . . ?
 Ni1 C8 C13 C14 -127.4(2) . . . . ?
 Ni1 C9 C10 C11 -55.1(2) . . . . ?
 Ni1 C10 C11 C12 -56.3(2) . . . . ?
 Ni1 C11 C12 C13 -56.7(2) . . . . ?
 Ni1 C12 C13 C8 -52.9(2) . . . . ?
 Ni1 C12 C13 C14 127.7(2) . . . . ?
 C1 C2 C3 Ni1 55.2(2) . . . . ?
 C1 C2 C3 C4 0.5(4) . . . . ?
 C2 C1 C6 Ni1 -55.7(2) . . . . ?
 C2 C1 C6 C5 -1.4(4) . . . . ?
 C2 C1 C6 C7 178.6(2) . . . . ?
 C2 C3 C4 Ni1 55.2(2) . . . . ?
 C2 C3 C4 C5 -0.3(4) . . . . ?
 C3 C4 C5 Ni1 56.2(2) . . . . ?
 C3 C4 C5 C6 -0.8(4) . . . . ?
 C4 C5 C6 Ni1 56.3(2) . . . . ?
 C4 C5 C6 C1 1.6(4) . . . . ?
 C4 C5 C6 C7 -178.4(2) . . . . ?
 C6 C1 C2 Ni1 55.8(2) . . . . ?
 C6 C1 C2 C3 0.4(4) . . . . ?
 C8 C9 C10 Ni1 56.4(2) . . . . ?
 C8 C9 C10 C11 1.3(4) . . . . ?
 C9 C8 C13 Ni1 -56.0(2) . . . . ?
 C9 C8 C13 C12 -2.8(4) . . . . ?
 C9 C8 C13 C14 176.6(2) . . . . ?
 C9 C10 C11 Ni1 54.9(2) . . . . ?
 C9 C10 C11 C12 -1.4(4) . . . . ?
 C10 C11 C12 Ni1 56.2(2) . . . . ?
 C10 C11 C12 C13 -0.6(4) . . . . ?
 C11 C12 C13 Ni1 55.5(2) . . . . ?
 C11 C12 C13 C8 2.7(4) . . . . ?
 C11 C12 C13 C14 -176.8(2) . . . . ?
 C13 C8 C9 Ni1 57.4(2) . . . . ?
 C13 C8 C9 C10 0.9(4) . . . . ?
 Cl1 B1 B2 Cl2 -1.2(3) . . . . ?
 Cl1 B1 B2 C15 110.5(2) . . . . ?
 Cl1 B1 B2 B3 143.2(2) . . . . ?
 Cl1 B1 B2 B6 -115.7(2) . . . . ?
 Cl1 B1 B2 B7 -153.54(19) . . . . ?
 Cl1 B1 B5 Cl5 0.2(3) . . . . ?
 Cl1 B1 B5 C15 -110.7(2) . . . . ?
 Cl1 B1 B5 B4 -143.6(2) . . . . ?
 Cl1 B1 B5 B9 152.6(2) . . . . ?
 Cl1 B1 B5 B10 114.8(2) . . . . ?
 Cl1 B1 B6 Cl6 -2.5(3) . . . . ?
 Cl1 B1 B6 B2 108.1(2) . . . . ?
 Cl1 B1 B6 B7 145.6(2) . . . . ?
 Cl1 B1 B6 B10 -113.6(2) . . . . ?
 Cl1 B1 B6 B11 -151.0(2) . . . . ?
 Cl1 B1 B10 Cl10 2.9(3) . . . . ?
 Cl1 B1 B10 B5 -107.6(2) . . . . ?
 Cl1 B1 B10 B6 114.9(2) . . . . ?
 Cl1 B1 B10 B9 -144.6(2) . . . . ?
 Cl1 B1 B10 B11 152.1(2) . . . . ?
 Cl2 B2 B3 Cl3 2.3(3) . . . . ?
 Cl2 B2 B3 C15 111.5(2) . . . . ?
 Cl2 B2 B3 B4 144.6(2) . . . . ?
 Cl2 B2 B3 B7 -114.8(2) . . . . ?
 Cl2 B2 B3 B8 -152.71(19) . . . . ?
 Cl2 B2 B6 Cl6 2.9(3) . . . . ?
 Cl2 B2 B6 B1 -107.9(2) . . . . ?
 Cl2 B2 B6 B7 114.0(2) . . . . ?
 Cl2 B2 B6 B10 -145.3(2) . . . . ?
 Cl2 B2 B6 B11 151.3(2) . . . . ?
 Cl2 B2 B7 Cl7 -2.2(3) . . . . ?
 Cl2 B2 B7 B3 108.3(2) . . . . ?
 Cl2 B2 B7 B6 -113.5(2) . . . . ?
 Cl2 B2 B7 B8 146.2(2) . . . . ?
 Cl2 B2 B7 B11 -150.7(2) . . . . ?
 Cl3 B3 B4 Cl4 -1.6(3) . . . . ?
 Cl3 B3 B4 C15 109.5(2) . . . . ?
 Cl3 B3 B4 B5 142.1(2) . . . . ?
 Cl3 B3 B4 B8 -117.2(2) . . . . ?
 Cl3 B3 B4 B9 -154.83(19) . . . . ?
 Cl3 B3 B7 Cl7 5.3(3) . . . . ?
 Cl3 B3 B7 B2 -107.0(2) . . . . ?
 Cl3 B3 B7 B6 -144.0(2) . . . . ?
 Cl3 B3 B7 B8 115.5(2) . . . . ?
 Cl3 B3 B7 B11 152.8(2) . . . . ?
 Cl3 B3 B8 Cl8 -4.7(3) . . . . ?
 Cl3 B3 B8 B4 106.5(2) . . . . ?
 Cl3 B3 B8 B7 -115.4(2) . . . . ?
 Cl3 B3 B8 B9 143.7(2) . . . . ?
 Cl3 B3 B8 B11 -152.8(2) . . . . ?
 Cl4 B4 B5 Cl5 0.5(3) . . . . ?
 Cl4 B4 B5 C15 111.1(2) . . . . ?
 Cl4 B4 B5 B1 143.9(2) . . . . ?
 Cl4 B4 B5 B9 -114.7(2) . . . . ?
 Cl4 B4 B5 B10 -152.54(19) . . . . ?
 Cl4 B4 B8 Cl8 2.9(3) . . . . ?
 Cl4 B4 B8 B3 -108.1(2) . . . . ?
 Cl4 B4 B8 B7 -145.5(2) . . . . ?
 Cl4 B4 B8 B9 113.5(2) . . . . ?
 Cl4 B4 B8 B11 151.2(2) . . . . ?
 Cl4 B4 B9 Cl9 -3.8(3) . . . . ?
 Cl4 B4 B9 B5 107.8(2) . . . . ?
 Cl4 B4 B9 B8 -114.5(2) . . . . ?
 Cl4 B4 B9 B10 144.9(2) . . . . ?
 Cl4 B4 B9 B11 -152.0(2) . . . . ?
 Cl5 B5 B9 Cl9 1.8(3) . . . . ?
 Cl5 B5 B9 B4 -108.4(3) . . . . ?
 Cl5 B5 B9 B8 -146.0(2) . . . . ?
 Cl5 B5 B9 B10 113.2(3) . . . . ?
 Cl5 B5 B9 B11 151.0(2) . . . . ?
 Cl5 B5 B10 Cl10 -4.4(3) . . . . ?
 Cl5 B5 B10 B1 107.1(2) . . . . ?
 Cl5 B5 B10 B6 144.6(2) . . . . ?
 Cl5 B5 B10 B9 -114.5(2) . . . . ?
 Cl5 B5 B10 B11 -152.4(2) . . . . ?
 Cl6 B6 B7 Cl7 -1.0(3) . . . . ?
 Cl6 B6 B7 B2 110.1(2) . . . . ?
 Cl6 B6 B7 B3 147.82(19) . . . . ?
 Cl6 B6 B7 B8 -148.84(19) . . . . ?
 Cl6 B6 B7 B11 -111.7(2) . . . . ?
 Cl6 B6 B10 Cl10 0.1(3) . . . . ?
 Cl6 B6 B10 B1 -110.3(2) . . . . ?
 Cl6 B6 B10 B5 -148.3(2) . . . . ?
 Cl6 B6 B10 B9 148.9(2) . . . . ?
 Cl6 B6 B10 B11 111.7(2) . . . . ?
 Cl6 B6 B11 Cl11 -1.1(3) . . . . ?
 Cl6 B6 B11 B7 110.6(2) . . . . ?
 Cl6 B6 B11 B8 148.04(19) . . . . ?
 Cl6 B6 B11 B9 -148.17(19) . . . . ?
 Cl6 B6 B11 B10 -110.7(2) . . . . ?
 Cl7 B7 B8 Cl8 -0.1(3) . . . . ?
 Cl7 B7 B8 B3 110.7(2) . . . . ?
 Cl7 B7 B8 B4 148.33(19) . . . . ?
 Cl7 B7 B8 B9 -148.34(19) . . . . ?
 Cl7 B7 B8 B11 -111.3(2) . . . . ?
 Cl7 B7 B11 Cl11 -2.2(3) . . . . ?
 Cl7 B7 B11 B6 -111.7(2) . . . . ?
 Cl7 B7 B11 B8 109.9(2) . . . . ?
 Cl7 B7 B11 B9 147.07(19) . . . . ?
 Cl7 B7 B11 B10 -148.97(19) . . . . ?
 Cl8 B8 B9 Cl9 0.9(3) . . . . ?
 Cl8 B8 B9 B4 110.9(2) . . . . ?
 Cl8 B8 B9 B5 148.9(2) . . . . ?
 Cl8 B8 B9 B10 -148.17(19) . . . . ?
 Cl8 B8 B9 B11 -111.3(2) . . . . ?
 Cl8 B8 B11 Cl11 0.1(3) . . . . ?
 Cl8 B8 B11 B6 -148.23(19) . . . . ?
 Cl8 B8 B11 B7 -110.7(2) . . . . ?
 Cl8 B8 B11 B9 110.6(2) . . . . ?
 Cl8 B8 B11 B10 147.82(19) . . . . ?
 Cl9 B9 B10 Cl10 0.5(3) . . . . ?
 Cl9 B9 B10 B1 148.3(2) . . . . ?
 Cl9 B9 B10 B5 110.8(2) . . . . ?
 Cl9 B9 B10 B6 -149.0(2) . . . . ?
 Cl9 B9 B10 B11 -111.9(2) . . . . ?
 Cl9 B9 B11 Cl11 2.1(3) . . . . ?
 Cl9 B9 B11 B6 148.72(19) . . . . ?
 Cl9 B9 B11 B7 -147.29(19) . . . . ?
 Cl9 B9 B11 B8 -110.1(2) . . . . ?
 Cl9 B9 B11 B10 111.2(2) . . . . ?
 Cl10 B10 B11 Cl11 1.7(3) . . . . ?
 Cl10 B10 B11 B6 111.9(2) . . . . ?
 Cl10 B10 B11 B7 149.18(19) . . . . ?
 Cl10 B10 B11 B8 -146.91(19) . . . . ?
 Cl10 B10 B11 B9 -109.7(2) . . . . ?
 C15 B1 B2 Cl2 -111.6(2) . . . . ?
 C15 B1 B2 B3 32.74(19) . . . . ?
 C15 B1 B2 B6 133.9(2) . . . . ?
 C15 B1 B2 B7 96.0(2) . . . . ?
 C15 B1 B5 Cl5 110.9(2) . . . . ?
 C15 B1 B5 B4 -32.96(19) . . . . ?
 C15 B1 B5 B9 -96.7(2) . . . . ?
 C15 B1 B5 B10 -134.5(2) . . . . ?
 C15 B1 B6 Cl6 -150.07(18) . . . . ?
 C15 B1 B6 B2 -39.43(18) . . . . ?
 C15 B1 B6 B7 -1.9(3) . . . . ?
 C15 B1 B6 B10 98.8(2) . . . . ?
 C15 B1 B6 B11 61.4(2) . . . . ?
 C15 B1 B10 Cl10 149.40(19) . . . . ?
 C15 B1 B10 B5 38.94(18) . . . . ?
 C15 B1 B10 B6 -98.6(2) . . . . ?
 C15 B1 B10 B9 1.9(3) . . . . ?
 C15 B1 B10 B11 -61.4(2) . . . . ?
 C15 B2 B3 Cl3 -109.2(2) . . . . ?
 C15 B2 B3 B4 33.08(19) . . . . ?
 C15 B2 B3 B7 133.7(2) . . . . ?
 C15 B2 B3 B8 95.8(2) . . . . ?
 C15 B2 B6 Cl6 150.33(19) . . . . ?
 C15 B2 B6 B1 39.46(18) . . . . ?
 C15 B2 B6 B7 -98.6(2) . . . . ?
 C15 B2 B6 B10 2.1(3) . . . . ?
 C15 B2 B6 B11 -61.3(2) . . . . ?
 C15 B2 B7 Cl7 -150.02(18) . . . . ?
 C15 B2 B7 B3 -39.55(18) . . . . ?
 C15 B2 B7 B6 98.7(2) . . . . ?
 C15 B2 B7 B8 -1.6(2) . . . . ?
 C15 B2 B7 B11 61.5(2) . . . . ?
 C15 B3 B4 Cl4 -111.1(2) . . . . ?
 C15 B3 B4 B5 32.58(19) . . . . ?
 C15 B3 B4 B8 133.2(2) . . . . ?
 C15 B3 B4 B9 95.7(2) . . . . ?
 C15 B3 B7 Cl7 151.48(18) . . . . ?
 C15 B3 B7 B2 39.24(18) . . . . ?
 C15 B3 B7 B6 2.2(2) . . . . ?
 C15 B3 B7 B8 -98.3(2) . . . . ?
 C15 B3 B7 B11 -60.9(2) . . . . ?
 C15 B3 B8 Cl8 -151.06(19) . . . . ?
 C15 B3 B8 B4 -39.90(18) . . . . ?
 C15 B3 B8 B7 98.2(2) . . . . ?
 C15 B3 B8 B9 -2.7(2) . . . . ?
 C15 B3 B8 B11 60.8(2) . . . . ?
 C15 B4 B5 Cl5 -110.5(2) . . . . ?
 C15 B4 B5 B1 32.82(19) . . . . ?
 C15 B4 B5 B9 134.2(2) . . . . ?
 C15 B4 B5 B10 96.4(2) . . . . ?
 C15 B4 B8 Cl8 150.93(18) . . . . ?
 C15 B4 B8 B3 39.91(18) . . . . ?
 C15 B4 B8 B7 2.6(2) . . . . ?
 C15 B4 B8 B9 -98.5(2) . . . . ?
 C15 B4 B8 B11 -60.8(2) . . . . ?
 C15 B4 B9 Cl9 -150.71(19) . . . . ?
 C15 B4 B9 B5 -39.03(18) . . . . ?
 C15 B4 B9 B8 98.6(2) . . . . ?
 C15 B4 B9 B10 -2.0(3) . . . . ?
 C15 B4 B9 B11 61.1(2) . . . . ?
 C15 B5 B9 Cl9 149.72(19) . . . . ?
 C15 B5 B9 B4 39.56(18) . . . . ?
 C15 B5 B9 B8 1.9(3) . . . . ?
 C15 B5 B9 B10 -98.8(2) . . . . ?
 C15 B5 B9 B11 -61.0(2) . . . . ?
 C15 B5 B10 Cl10 -150.64(19) . . . . ?
 C15 B5 B10 B1 -39.10(18) . . . . ?
 C15 B5 B10 B6 -1.6(3) . . . . ?
 C15 B5 B10 B9 99.3(2) . . . . ?
 C15 B5 B10 B11 61.4(2) . . . . ?
 B1 C15 B2 Cl2 108.3(2) . . . . ?
 B1 C15 B2 B3 -143.0(2) . . . . ?
 B1 C15 B2 B6 -39.93(19) . . . . ?
 B1 C15 B2 B7 -102.9(2) . . . . ?
 B1 C15 B3 Cl3 145.1(2) . . . . ?
 B1 C15 B3 B2 36.2(2) . . . . ?
 B1 C15 B3 B4 -106.3(2) . . . . ?
 B1 C15 B3 B7 -3.7(3) . . . . ?
 B1 C15 B3 B8 -66.0(2) . . . . ?
 B1 C15 B4 Cl4 -144.5(2) . . . . ?
 B1 C15 B4 B3 106.8(2) . . . . ?
 B1 C15 B4 B5 -36.2(2) . . . . ?
 B1 C15 B4 B8 66.2(2) . . . . ?
 B1 C15 B4 B9 3.5(3) . . . . ?
 B1 C15 B5 Cl5 -107.7(2) . . . . ?
 B1 C15 B5 B4 143.0(2) . . . . ?
 B1 C15 B5 B9 103.0(2) . . . . ?
 B1 C15 B5 B10 39.69(19) . . . . ?
 B1 B2 B3 Cl3 -141.9(2) . . . . ?
 B1 B2 B3 C15 -32.75(19) . . . . ?
 B1 B2 B3 B4 0.3(3) . . . . ?
 B1 B2 B3 B7 101.0(2) . . . . ?
 B1 B2 B3 B8 63.0(3) . . . . ?
 B1 B2 B6 Cl6 110.9(2) . . . . ?
 B1 B2 B6 B7 -138.1(2) . . . . ?
 B1 B2 B6 B10 -37.34(19) . . . . ?
 B1 B2 B6 B11 -100.7(2) . . . . ?
 B1 B2 B7 Cl7 148.70(19) . . . . ?
 B1 B2 B7 B3 -100.8(2) . . . . ?
 B1 B2 B7 B6 37.37(19) . . . . ?
 B1 B2 B7 B8 -62.9(2) . . . . ?
 B1 B2 B7 B11 0.2(3) . . . . ?
 B1 B5 B9 Cl9 -148.8(2) . . . . ?
 B1 B5 B9 B4 101.1(2) . . . . ?
 B1 B5 B9 B8 63.4(3) . . . . ?
 B1 B5 B9 B10 -37.34(19) . . . . ?
 B1 B5 B9 B11 0.5(3) . . . . ?
 B1 B5 B10 Cl10 -111.5(2) . . . . ?
 B1 B5 B10 B6 37.51(19) . . . . ?
 B1 B5 B10 B9 138.4(2) . . . . ?
 B1 B5 B10 B11 100.5(2) . . . . ?
 B1 B6 B7 Cl7 -149.02(19) . . . . ?
 B1 B6 B7 B2 -37.82(19) . . . . ?
 B1 B6 B7 B3 -0.2(3) . . . . ?
 B1 B6 B7 B8 63.2(2) . . . . ?
 B1 B6 B7 B11 100.3(2) . . . . ?
 B1 B6 B10 Cl10 110.4(2) . . . . ?
 B1 B6 B10 B5 -38.02(19) . . . . ?
 B1 B6 B10 B9 -100.8(2) . . . . ?
 B1 B6 B10 B11 -138.0(2) . . . . ?
 B1 B6 B11 Cl11 146.97(19) . . . . ?
 B1 B6 B11 B7 -101.3(2) . . . . ?
 B1 B6 B11 B8 -63.9(2) . . . . ?
 B1 B6 B11 B9 -0.1(3) . . . . ?
 B1 B6 B11 B10 37.37(19) . . . . ?
 B1 B10 B11 Cl11 -147.22(19) . . . . ?
 B1 B10 B11 B6 -37.03(19) . . . . ?
 B1 B10 B11 B7 0.2(3) . . . . ?
 B1 B10 B11 B8 64.1(2) . . . . ?
 B1 B10 B11 B9 101.3(2) . . . . ?
 B2 C15 B1 Cl1 -109.1(2) . . . . ?
 B2 C15 B1 B5 142.6(2) . . . . ?
 B2 C15 B1 B6 40.00(19) . . . . ?
 B2 C15 B1 B10 103.0(2) . . . . ?
 B2 C15 B3 Cl3 108.8(2) . . . . ?
 B2 C15 B3 B4 -142.5(2) . . . . ?
 B2 C15 B3 B7 -39.91(18) . . . . ?
 B2 C15 B3 B8 -102.2(2) . . . . ?
 B2 C15 B4 Cl4 145.5(2) . . . . ?
 B2 C15 B4 B3 36.8(2) . . . . ?
 B2 C15 B4 B5 -106.2(2) . . . . ?
 B2 C15 B4 B8 -3.9(3) . . . . ?
 B2 C15 B4 B9 -66.6(2) . . . . ?
 B2 C15 B5 Cl5 -144.2(2) . . . . ?
 B2 C15 B5 B1 -36.5(2) . . . . ?
 B2 C15 B5 B4 106.5(2) . . . . ?
 B2 C15 B5 B9 66.5(3) . . . . ?
 B2 C15 B5 B10 3.2(3) . . . . ?
 B2 B1 B5 Cl5 143.9(2) . . . . ?
 B2 B1 B5 C15 33.02(19) . . . . ?
 B2 B1 B5 B4 0.1(3) . . . . ?
 B2 B1 B5 B9 -63.7(3) . . . . ?
 B2 B1 B5 B10 -101.4(2) . . . . ?
 B2 B1 B6 Cl6 -110.6(2) . . . . ?
 B2 B1 B6 B7 37.49(19) . . . . ?
 B2 B1 B6 B10 138.3(2) . . . . ?
 B2 B1 B6 B11 100.9(2) . . . . ?
 B2 B1 B10 Cl10 -149.33(19) . . . . ?
 B2 B1 B10 B5 100.2(2) . . . . ?
 B2 B1 B10 B6 -37.33(19) . . . . ?
 B2 B1 B10 B9 63.2(2) . . . . ?
 B2 B1 B10 B11 -0.1(3) . . . . ?
 B2 B3 B4 Cl4 -143.9(2) . . . . ?
 B2 B3 B4 C15 -32.87(19) . . . . ?
 B2 B3 B4 B5 -0.3(3) . . . . ?
 B2 B3 B4 B8 100.4(2) . . . . ?
 B2 B3 B4 B9 62.8(2) . . . . ?
 B2 B3 B7 Cl7 112.2(2) . . . . ?
 B2 B3 B7 B6 -37.07(18) . . . . ?
 B2 B3 B7 B8 -137.6(2) . . . . ?
 B2 B3 B7 B11 -100.2(2) . . . . ?
 B2 B3 B8 Cl8 148.33(19) . . . . ?
 B2 B3 B8 B4 -100.5(2) . . . . ?
 B2 B3 B8 B7 37.61(18) . . . . ?
 B2 B3 B8 B9 -63.3(2) . . . . ?
 B2 B3 B8 B11 0.2(3) . . . . ?
 B2 B6 B7 Cl7 -111.2(2) . . . . ?
 B2 B6 B7 B3 37.67(19) . . . . ?
 B2 B6 B7 B8 101.0(2) . . . . ?
 B2 B6 B7 B11 138.1(2) . . . . ?
 B2 B6 B10 Cl10 148.1(2) . . . . ?
 B2 B6 B10 B1 37.68(19) . . . . ?
 B2 B6 B10 B5 -0.3(3) . . . . ?
 B2 B6 B10 B9 -63.1(3) . . . . ?
 B2 B6 B10 B11 -100.3(2) . . . . ?
 B2 B6 B11 Cl11 -149.03(19) . . . . ?
 B2 B6 B11 B7 -37.33(19) . . . . ?
 B2 B6 B11 B8 0.1(3) . . . . ?
 B2 B6 B11 B9 63.9(2) . . . . ?
 B2 B6 B11 B10 101.4(2) . . . . ?
 B2 B7 B8 Cl8 -149.02(19) . . . . ?
 B2 B7 B8 B3 -38.27(18) . . . . ?
 B2 B7 B8 B4 -0.6(3) . . . . ?
 B2 B7 B8 B9 62.7(2) . . . . ?
 B2 B7 B8 B11 99.8(2) . . . . ?
 B2 B7 B11 Cl11 146.51(19) . . . . ?
 B2 B7 B11 B6 36.95(19) . . . . ?
 B2 B7 B11 B8 -101.4(2) . . . . ?
 B2 B7 B11 B9 -64.2(2) . . . . ?
 B2 B7 B11 B10 -0.3(3) . . . . ?
 B3 C15 B1 Cl1 -145.5(2) . . . . ?
 B3 C15 B1 B2 -36.4(2) . . . . ?
 B3 C15 B1 B5 106.2(2) . . . . ?
 B3 C15 B1 B6 3.6(3) . . . . ?
 B3 C15 B1 B10 66.7(2) . . . . ?
 B3 C15 B2 Cl2 -108.7(2) . . . . ?
 B3 C15 B2 B1 143.0(2) . . . . ?
 B3 C15 B2 B6 103.1(2) . . . . ?
 B3 C15 B2 B7 40.11(18) . . . . ?
 B3 C15 B4 Cl4 108.7(2) . . . . ?
 B3 C15 B4 B5 -143.0(2) . . . . ?
 B3 C15 B4 B8 -40.66(18) . . . . ?
 B3 C15 B4 B9 -103.3(2) . . . . ?
 B3 C15 B5 Cl5 145.4(2) . . . . ?
 B3 C15 B5 B1 -106.9(2) . . . . ?
 B3 C15 B5 B4 36.1(2) . . . . ?
 B3 C15 B5 B9 -4.0(3) . . . . ?
 B3 C15 B5 B10 -67.2(3) . . . . ?
 B3 B2 B6 Cl6 -148.41(19) . . . . ?
 B3 B2 B6 B1 100.7(2) . . . . ?
 B3 B2 B6 B7 -37.36(19) . . . . ?
 B3 B2 B6 B10 63.4(2) . . . . ?
 B3 B2 B6 B11 0.0(3) . . . . ?
 B3 B2 B7 Cl7 -110.5(2) . . . . ?
 B3 B2 B7 B6 138.2(2) . . . . ?
 B3 B2 B7 B8 37.94(18) . . . . ?
 B3 B2 B7 B11 101.1(2) . . . . ?
 B3 B4 B5 Cl5 -143.2(2) . . . . ?
 B3 B4 B5 C15 -32.68(19) . . . . ?
 B3 B4 B5 B1 0.1(3) . . . . ?
 B3 B4 B5 B9 101.5(2) . . . . ?
 B3 B4 B5 B10 63.7(3) . . . . ?
 B3 B4 B8 Cl8 111.0(2) . . . . ?
 B3 B4 B8 B7 -37.35(18) . . . . ?
 B3 B4 B8 B9 -138.4(2) . . . . ?
 B3 B4 B8 B11 -100.7(2) . . . . ?
 B3 B4 B9 Cl9 148.09(19) . . . . ?
 B3 B4 B9 B5 -100.2(2) . . . . ?
 B3 B4 B9 B8 37.39(19) . . . . ?
 B3 B4 B9 B10 -63.2(2) . . . . ?
 B3 B4 B9 B11 -0.1(3) . . . . ?
 B3 B7 B8 Cl8 -110.8(2) . . . . ?
 B3 B7 B8 B4 37.66(19) . . . . ?
 B3 B7 B8 B9 101.0(2) . . . . ?
 B3 B7 B8 B11 138.0(2) . . . . ?
 B3 B7 B11 Cl11 -149.53(19) . . . . ?
 B3 B7 B11 B6 100.9(2) . . . . ?
 B3 B7 B11 B8 -37.43(19) . . . . ?
 B3 B7 B11 B9 -0.3(3) . . . . ?
 B3 B7 B11 B10 63.7(2) . . . . ?
 B3 B8 B9 Cl9 -147.5(2) . . . . ?
 B3 B8 B9 B4 -37.47(19) . . . . ?
 B3 B8 B9 B5 0.5(3) . . . . ?
 B3 B8 B9 B10 63.4(2) . . . . ?
 B3 B8 B9 B11 100.3(2) . . . . ?
 B3 B8 B11 Cl11 148.17(19) . . . . ?
 B3 B8 B11 B6 -0.2(3) . . . . ?
 B3 B8 B11 B7 37.32(19) . . . . ?
 B3 B8 B11 B9 -101.4(2) . . . . ?
 B3 B8 B11 B10 -64.1(2) . . . . ?
 B4 C15 B1 Cl1 144.4(2) . . . . ?
 B4 C15 B1 B2 -106.5(2) . . . . ?
 B4 C15 B1 B5 36.1(2) . . . . ?
 B4 C15 B1 B6 -66.5(2) . . . . ?
 B4 C15 B1 B10 -3.4(3) . . . . ?
 B4 C15 B2 Cl2 -145.3(2) . . . . ?
 B4 C15 B2 B1 106.4(2) . . . . ?
 B4 C15 B2 B3 -36.6(2) . . . . ?
 B4 C15 B2 B6 66.5(2) . . . . ?
 B4 C15 B2 B7 3.5(3) . . . . ?
 B4 C15 B3 Cl3 -108.7(2) . . . . ?
 B4 C15 B3 B2 142.5(2) . . . . ?
 B4 C15 B3 B7 102.6(2) . . . . ?
 B4 C15 B3 B8 40.28(18) . . . . ?
 B4 C15 B5 Cl5 109.3(2) . . . . ?
 B4 C15 B5 B1 -143.0(2) . . . . ?
 B4 C15 B5 B9 -40.04(19) . . . . ?
 B4 C15 B5 B10 -103.3(2) . . . . ?
 B4 B3 B7 Cl7 -147.36(19) . . . . ?
 B4 B3 B7 B2 100.4(2) . . . . ?
 B4 B3 B7 B6 63.3(2) . . . . ?
 B4 B3 B7 B8 -37.16(18) . . . . ?
 B4 B3 B7 B11 0.2(3) . . . . ?
 B4 B3 B8 Cl8 -111.2(2) . . . . ?
 B4 B3 B8 B7 138.1(2) . . . . ?
 B4 B3 B8 B9 37.20(19) . . . . ?
 B4 B3 B8 B11 100.7(2) . . . . ?
 B4 B5 B9 Cl9 110.2(2) . . . . ?
 B4 B5 B9 B8 -37.62(19) . . . . ?
 B4 B5 B9 B10 -138.4(2) . . . . ?
 B4 B5 B9 B11 -100.6(2) . . . . ?
 B4 B5 B10 Cl10 147.5(2) . . . . ?
 B4 B5 B10 B1 -100.9(2) . . . . ?
 B4 B5 B10 B6 -63.4(3) . . . . ?
 B4 B5 B10 B9 37.42(19) . . . . ?
 B4 B5 B10 B11 -0.5(3) . . . . ?
 B4 B8 B9 Cl9 -110.0(2) . . . . ?
 B4 B8 B9 B5 37.97(19) . . . . ?
 B4 B8 B9 B10 100.9(2) . . . . ?
 B4 B8 B9 B11 137.8(2) . . . . ?
 B4 B8 B11 Cl11 -148.05(19) . . . . ?
 B4 B8 B11 B6 63.6(2) . . . . ?
 B4 B8 B11 B7 101.1(2) . . . . ?
 B4 B8 B11 B9 -37.59(19) . . . . ?
 B4 B8 B11 B10 -0.4(3) . . . . ?
 B4 B9 B10 Cl10 -147.8(2) . . . . ?
 B4 B9 B10 B1 0.1(3) . . . . ?
 B4 B9 B10 B5 -37.39(19) . . . . ?
 B4 B9 B10 B6 62.8(3) . . . . ?
 B4 B9 B10 B11 99.9(2) . . . . ?
 B4 B9 B11 Cl11 149.59(19) . . . . ?
 B4 B9 B11 B6 -63.8(2) . . . . ?
 B4 B9 B11 B7 0.2(3) . . . . ?
 B4 B9 B11 B8 37.40(19) . . . . ?
 B4 B9 B11 B10 -101.2(2) . . . . ?
 B5 C15 B1 Cl1 108.3(2) . . . . ?
 B5 C15 B1 B2 -142.6(2) . . . . ?
 B5 C15 B1 B6 -102.6(2) . . . . ?
 B5 C15 B1 B10 -39.51(19) . . . . ?
 B5 C15 B2 Cl2 144.9(2) . . . . ?
 B5 C15 B2 B1 36.6(2) . . . . ?
 B5 C15 B2 B3 -106.5(2) . . . . ?
 B5 C15 B2 B6 -3.4(3) . . . . ?
 B5 C15 B2 B7 -66.4(2) . . . . ?
 B5 C15 B3 Cl3 -144.7(2) . . . . ?
 B5 C15 B3 B2 106.5(2) . . . . ?
 B5 C15 B3 B4 -36.1(2) . . . . ?
 B5 C15 B3 B7 66.5(2) . . . . ?
 B5 C15 B3 B8 4.2(3) . . . . ?
 B5 C15 B4 Cl4 -108.3(2) . . . . ?
 B5 C15 B4 B3 143.0(2) . . . . ?
 B5 C15 B4 B8 102.3(2) . . . . ?
 B5 C15 B4 B9 39.63(19) . . . . ?
 B5 B1 B2 Cl2 -144.6(2) . . . . ?
 B5 B1 B2 C15 -32.98(19) . . . . ?
 B5 B1 B2 B3 -0.2(3) . . . . ?
 B5 B1 B2 B6 100.9(2) . . . . ?
 B5 B1 B2 B7 63.0(3) . . . . ?
 B5 B1 B6 Cl6 148.87(19) . . . . ?
 B5 B1 B6 B2 -100.5(2) . . . . ?
 B5 B1 B6 B7 -63.0(2) . . . . ?
 B5 B1 B6 B10 37.78(19) . . . . ?
 B5 B1 B6 B11 0.4(3) . . . . ?
 B5 B1 B10 Cl10 110.5(2) . . . . ?
 B5 B1 B10 B6 -137.5(2) . . . . ?
 B5 B1 B10 B9 -37.04(19) . . . . ?
 B5 B1 B10 B11 -100.3(2) . . . . ?
 B5 B4 B8 Cl8 -148.21(19) . . . . ?
 B5 B4 B8 B3 100.8(2) . . . . ?
 B5 B4 B8 B7 63.4(2) . . . . ?
 B5 B4 B8 B9 -37.63(19) . . . . ?
 B5 B4 B8 B11 0.1(3) . . . . ?
 B5 B4 B9 Cl9 -111.7(2) . . . . ?
 B5 B4 B9 B8 137.6(2) . . . . ?
 B5 B4 B9 B10 37.04(19) . . . . ?
 B5 B4 B9 B11 100.1(2) . . . . ?
 B5 B9 B10 Cl10 -110.4(2) . . . . ?
 B5 B9 B10 B1 37.46(19) . . . . ?
 B5 B9 B10 B6 100.2(2) . . . . ?
 B5 B9 B10 B11 137.3(2) . . . . ?
 B5 B9 B11 Cl11 -146.88(19) . . . . ?
 B5 B9 B11 B6 -0.2(3) . . . . ?
 B5 B9 B11 B7 63.8(2) . . . . ?
 B5 B9 B11 B8 100.9(2) . . . . ?
 B5 B9 B11 B10 -37.71(19) . . . . ?
 B5 B10 B11 Cl11 149.15(19) . . . . ?
 B5 B10 B11 B6 -100.7(2) . . . . ?
 B5 B10 B11 B7 -63.4(2) . . . . ?
 B5 B10 B11 B8 0.5(3) . . . . ?
 B5 B10 B11 B9 37.70(19) . . . . ?
 B6 B1 B2 Cl2 114.5(2) . . . . ?
 B6 B1 B2 C15 -133.9(2) . . . . ?
 B6 B1 B2 B3 -101.2(2) . . . . ?
 B6 B1 B2 B7 -37.89(19) . . . . ?
 B6 B1 B5 Cl5 -152.9(2) . . . . ?
 B6 B1 B5 C15 96.2(2) . . . . ?
 B6 B1 B5 B4 63.2(3) . . . . ?
 B6 B1 B5 B9 -0.5(3) . . . . ?
 B6 B1 B5 B10 -38.31(19) . . . . ?
 B6 B1 B10 Cl10 -112.0(2) . . . . ?
 B6 B1 B10 B5 137.5(2) . . . . ?
 B6 B1 B10 B9 100.5(2) . . . . ?
 B6 B1 B10 B11 37.24(19) . . . . ?
 B6 B2 B3 Cl3 154.92(19) . . . . ?
 B6 B2 B3 C15 -95.9(2) . . . . ?
 B6 B2 B3 B4 -62.8(2) . . . . ?
 B6 B2 B3 B7 37.83(19) . . . . ?
 B6 B2 B3 B8 -0.1(3) . . . . ?
 B6 B2 B7 Cl7 111.3(2) . . . . ?
 B6 B2 B7 B3 -138.2(2) . . . . ?
 B6 B2 B7 B8 -100.3(2) . . . . ?
 B6 B2 B7 B11 -37.14(18) . . . . ?
 B6 B7 B8 Cl8 148.28(19) . . . . ?
 B6 B7 B8 B3 -101.0(2) . . . . ?
 B6 B7 B8 B4 -63.3(2) . . . . ?
 B6 B7 B8 B9 0.0(3) . . . . ?
 B6 B7 B8 B11 37.07(19) . . . . ?
 B6 B7 B11 Cl11 109.6(2) . . . . ?
 B6 B7 B11 B8 -138.3(2) . . . . ?
 B6 B7 B11 B9 -101.2(2) . . . . ?
 B6 B7 B11 B10 -37.24(19) . . . . ?
 B6 B10 B11 Cl11 -110.2(2) . . . . ?
 B6 B10 B11 B7 37.27(19) . . . . ?
 B6 B10 B11 B8 101.2(2) . . . . ?
 B6 B10 B11 B9 138.4(2) . . . . ?
 B7 B2 B3 Cl3 117.1(2) . . . . ?
 B7 B2 B3 C15 -133.7(2) . . . . ?
 B7 B2 B3 B4 -100.7(2) . . . . ?
 B7 B2 B3 B8 -37.94(18) . . . . ?
 B7 B2 B6 Cl6 -111.0(2) . . . . ?
 B7 B2 B6 B1 138.1(2) . . . . ?
 B7 B2 B6 B10 100.7(2) . . . . ?
 B7 B2 B6 B11 37.36(18) . . . . ?
 B7 B3 B4 Cl4 153.20(19) . . . . ?
 B7 B3 B4 C15 -95.7(2) . . . . ?
 B7 B3 B4 B5 -63.1(2) . . . . ?
 B7 B3 B4 B8 37.52(18) . . . . ?
 B7 B3 B4 B9 -0.1(3) . . . . ?
 B7 B3 B8 Cl8 110.7(2) . . . . ?
 B7 B3 B8 B4 -138.1(2) . . . . ?
 B7 B3 B8 B9 -100.9(2) . . . . ?
 B7 B3 B8 B11 -37.42(19) . . . . ?
 B7 B6 B10 Cl10 -148.5(2) . . . . ?
 B7 B6 B10 B1 101.1(2) . . . . ?
 B7 B6 B10 B5 63.1(3) . . . . ?
 B7 B6 B10 B9 0.3(3) . . . . ?
 B7 B6 B10 B11 -36.94(19) . . . . ?
 B7 B6 B11 Cl11 -111.7(2) . . . . ?
 B7 B6 B11 B8 37.46(19) . . . . ?
 B7 B6 B11 B9 101.2(2) . . . . ?
 B7 B6 B11 B10 138.7(2) . . . . ?
 B7 B8 B9 Cl9 149.23(19) . . . . ?
 B7 B8 B9 B4 -100.8(2) . . . . ?
 B7 B8 B9 B5 -62.8(2) . . . . ?
 B7 B8 B9 B10 0.1(3) . . . . ?
 B7 B8 B9 B11 37.01(19) . . . . ?
 B7 B8 B11 Cl11 110.8(2) . . . . ?
 B7 B8 B11 B6 -37.51(19) . . . . ?
 B7 B8 B11 B9 -138.7(2) . . . . ?
 B7 B8 B11 B10 -101.5(2) . . . . ?
 B8 B3 B4 Cl4 115.7(2) . . . . ?
 B8 B3 B4 C15 -133.2(2) . . . . ?
 B8 B3 B4 B5 -100.7(2) . . . . ?
 B8 B3 B4 B9 -37.59(19) . . . . ?
 B8 B3 B7 Cl7 -110.2(2) . . . . ?
 B8 B3 B7 B2 137.6(2) . . . . ?
 B8 B3 B7 B6 100.5(2) . . . . ?
 B8 B3 B7 B11 37.37(18) . . . . ?
 B8 B4 B5 Cl5 153.34(19) . . . . ?
 B8 B4 B5 C15 -96.1(2) . . . . ?
 B8 B4 B5 B1 -63.3(3) . . . . ?
 B8 B4 B5 B9 38.06(19) . . . . ?
 B8 B4 B5 B10 0.3(3) . . . . ?
 B8 B4 B9 Cl9 110.7(2) . . . . ?
 B8 B4 B9 B5 -137.6(2) . . . . ?
 B8 B4 B9 B10 -100.6(2) . . . . ?
 B8 B4 B9 B11 -37.49(19) . . . . ?
 B8 B7 B11 Cl11 -112.1(2) . . . . ?
 B8 B7 B11 B6 138.3(2) . . . . ?
 B8 B7 B11 B9 37.14(19) . . . . ?
 B8 B7 B11 B10 101.1(2) . . . . ?
 B8 B9 B10 Cl10 149.21(19) . . . . ?
 B8 B9 B10 B1 -63.0(2) . . . . ?
 B8 B9 B10 B5 -100.4(2) . . . . ?
 B8 B9 B10 B6 -0.2(3) . . . . ?
 B8 B9 B10 B11 36.88(19) . . . . ?
 B8 B9 B11 Cl11 112.2(2) . . . . ?
 B8 B9 B11 B6 -101.2(2) . . . . ?
 B8 B9 B11 B7 -37.17(19) . . . . ?
 B8 B9 B11 B10 -138.6(2) . . . . ?
 B9 B4 B5 Cl5 115.3(2) . . . . ?
 B9 B4 B5 C15 -134.2(2) . . . . ?
 B9 B4 B5 B1 -101.4(2) . . . . ?
 B9 B4 B5 B10 -37.80(19) . . . . ?
 B9 B4 B8 Cl8 -110.6(2) . . . . ?
 B9 B4 B8 B3 138.4(2) . . . . ?
 B9 B4 B8 B7 101.0(2) . . . . ?
 B9 B4 B8 B11 37.69(19) . . . . ?
 B9 B5 B10 Cl10 110.1(2) . . . . ?
 B9 B5 B10 B1 -138.4(2) . . . . ?
 B9 B5 B10 B6 -100.9(2) . . . . ?
 B9 B5 B10 B11 -37.91(19) . . . . ?
 B9 B8 B11 Cl11 -110.5(2) . . . . ?
 B9 B8 B11 B6 101.2(2) . . . . ?
 B9 B8 B11 B7 138.7(2) . . . . ?
 B9 B8 B11 B10 37.22(19) . . . . ?
 B9 B10 B11 Cl11 111.4(2) . . . . ?
 B9 B10 B11 B6 -138.4(2) . . . . ?
 B9 B10 B11 B7 -101.1(2) . . . . ?
 B9 B10 B11 B8 -37.18(19) . . . . ?
 B10 B1 B2 Cl2 152.28(19) . . . . ?
 B10 B1 B2 C15 -96.1(2) . . . . ?
 B10 B1 B2 B3 -63.4(3) . . . . ?
 B10 B1 B2 B6 37.80(19) . . . . ?
 B10 B1 B2 B7 -0.1(3) . . . . ?
 B10 B1 B5 Cl5 -114.6(2) . . . . ?
 B10 B1 B5 C15 134.5(2) . . . . ?
 B10 B1 B5 B4 101.5(2) . . . . ?
 B10 B1 B5 B9 37.79(19) . . . . ?
 B10 B1 B6 Cl6 111.1(2) . . . . ?
 B10 B1 B6 B2 -138.3(2) . . . . ?
 B10 B1 B6 B7 -100.8(2) . . . . ?
 B10 B1 B6 B11 -37.41(18) . . . . ?
 B10 B5 B9 Cl9 -111.4(2) . . . . ?
 B10 B5 B9 B4 138.4(2) . . . . ?
 B10 B5 B9 B8 100.8(2) . . . . ?
 B10 B5 B9 B11 37.80(18) . . . . ?
 B10 B6 B7 Cl7 147.62(19) . . . . ?
 B10 B6 B7 B2 -101.2(2) . . . . ?
 B10 B6 B7 B3 -63.5(2) . . . . ?
 B10 B6 B7 B8 -0.2(3) . . . . ?
 B10 B6 B7 B11 36.93(19) . . . . ?
 B10 B6 B11 Cl11 109.6(2) . . . . ?
 B10 B6 B11 B7 -138.7(2) . . . . ?
 B10 B6 B11 B8 -101.3(2) . . . . ?
 B10 B6 B11 B9 -37.46(19) . . . . ?
 B10 B9 B11 Cl11 -109.2(2) . . . . ?
 B10 B9 B11 B6 37.48(18) . . . . ?
 B10 B9 B11 B7 101.5(2) . . . . ?
 B10 B9 B11 B8 138.6(2) . . . . ?
 B11 B6 B7 Cl7 110.7(2) . . . . ?
 B11 B6 B7 B2 -138.1(2) . . . . ?
 B11 B6 B7 B3 -100.5(2) . . . . ?
 B11 B6 B7 B8 -37.11(19) . . . . ?
 B11 B6 B10 Cl10 -111.6(2) . . . . ?
 B11 B6 B10 B1 138.0(2) . . . . ?
 B11 B6 B10 B5 100.0(2) . . . . ?
 B11 B6 B10 B9 37.20(19) . . . . ?
 B11 B7 B8 Cl8 111.2(2) . . . . ?
 B11 B7 B8 B3 -138.0(2) . . . . ?
 B11 B7 B8 B4 -100.4(2) . . . . ?
 B11 B7 B8 B9 -37.05(19) . . . . ?
 B11 B8 B9 Cl9 112.2(2) . . . . ?
 B11 B8 B9 B4 -137.8(2) . . . . ?
 B11 B8 B9 B5 -99.8(2) . . . . ?
 B11 B8 B9 B10 -36.87(19) . . . . ?
 B11 B9 B10 Cl10 112.3(2) . . . . ?
 B11 B9 B10 B1 -99.8(2) . . . . ?
 B11 B9 B10 B5 -137.3(2) . . . . ?
 B11 B9 B10 B6 -37.12(19) . . . . ?
 Cl12 B12 B13 Cl13 0.6(3) . . . . ?
 Cl12 B12 B13 C16 -110.6(2) . . . . ?
 Cl12 B12 B13 B14 -143.62(19) . . . . ?
 Cl12 B12 B13 B18 115.4(2) . . . . ?
 Cl12 B12 B13 B19 153.21(19) . . . . ?
 Cl12 B12 B16 Cl16 -1.0(3) . . . . ?
 Cl12 B12 B16 C16 110.6(2) . . . . ?
 Cl12 B12 B16 B15 143.28(19) . . . . ?
 Cl12 B12 B16 B17 -115.6(2) . . . . ?
 Cl12 B12 B16 B21 -153.63(19) . . . . ?
 Cl12 B12 B17 Cl17 -2.8(3) . . . . ?
 Cl12 B12 B17 B16 107.5(2) . . . . ?
 Cl12 B12 B17 B18 -114.2(2) . . . . ?
 Cl12 B12 B17 B21 144.8(2) . . . . ?
 Cl12 B12 B17 B22 -151.9(2) . . . . ?
 Cl12 B12 B18 Cl18 1.1(3) . . . . ?
 Cl12 B12 B18 B13 -107.8(2) . . . . ?
 Cl12 B12 B18 B17 114.2(2) . . . . ?
 Cl12 B12 B18 B19 -145.3(2) . . . . ?
 Cl12 B12 B18 B22 151.7(2) . . . . ?
 Cl13 B13 B14 Cl14 -0.3(3) . . . . ?
 Cl13 B13 B14 C16 -111.0(2) . . . . ?
 Cl13 B13 B14 B15 -143.4(2) . . . . ?
 Cl13 B13 B14 B19 115.1(2) . . . . ?
 Cl13 B13 B14 B20 152.71(19) . . . . ?
 Cl13 B13 B18 Cl18 -2.0(3) . . . . ?
 Cl13 B13 B18 B12 107.9(2) . . . . ?
 Cl13 B13 B18 B17 145.4(2) . . . . ?
 Cl13 B13 B18 B19 -114.1(2) . . . . ?
 Cl13 B13 B18 B22 -151.5(2) . . . . ?
 Cl13 B13 B19 Cl19 2.6(3) . . . . ?
 Cl13 B13 B19 B14 -108.5(2) . . . . ?
 Cl13 B13 B19 B18 113.8(2) . . . . ?
 Cl13 B13 B19 B20 -145.1(2) . . . . ?
 Cl13 B13 B19 B22 151.4(2) . . . . ?
 Cl14 B14 B15 Cl15 1.2(3) . . . . ?
 Cl14 B14 B15 C16 -109.8(2) . . . . ?
 Cl14 B14 B15 B16 -142.93(19) . . . . ?
 Cl14 B14 B15 B20 116.2(2) . . . . ?
 Cl14 B14 B15 B21 154.68(18) . . . . ?
 Cl14 B14 B19 Cl19 -4.8(3) . . . . ?
 Cl14 B14 B19 B13 106.1(2) . . . . ?
 Cl14 B14 B19 B18 143.6(2) . . . . ?
 Cl14 B14 B19 B20 -115.3(2) . . . . ?
 Cl14 B14 B19 B22 -153.08(19) . . . . ?
 Cl14 B14 B20 Cl20 2.3(3) . . . . ?
 Cl14 B14 B20 B15 -108.1(2) . . . . ?
 Cl14 B14 B20 B19 113.5(2) . . . . ?
 Cl14 B14 B20 B21 -146.0(2) . . . . ?
 Cl14 B14 B20 B22 151.09(19) . . . . ?
 Cl15 B15 B16 Cl16 -0.6(3) . . . . ?
 Cl15 B15 B16 C16 -111.2(2) . . . . ?
 Cl15 B15 B16 B12 -143.93(19) . . . . ?
 Cl15 B15 B16 B17 152.65(18) . . . . ?
 Cl15 B15 B16 B21 115.2(2) . . . . ?
 Cl15 B15 B20 Cl20 -3.4(3) . . . . ?
 Cl15 B15 B20 B14 108.7(2) . . . . ?
 Cl15 B15 B20 B19 145.9(2) . . . . ?
 Cl15 B15 B20 B21 -114.3(2) . . . . ?
 Cl15 B15 B20 B22 -151.20(19) . . . . ?
 Cl15 B15 B21 Cl21 4.5(3) . . . . ?
 Cl15 B15 B21 B16 -107.6(2) . . . . ?
 Cl15 B15 B21 B17 -145.0(2) . . . . ?
 Cl15 B15 B21 B20 114.2(2) . . . . ?
 Cl15 B15 B21 B22 151.5(2) . . . . ?
 Cl16 B16 B17 Cl17 5.0(3) . . . . ?
 Cl16 B16 B17 B12 -106.8(2) . . . . ?
 Cl16 B16 B17 B18 -143.9(2) . . . . ?
 Cl16 B16 B17 B21 115.4(2) . . . . ?
 Cl16 B16 B17 B22 152.66(19) . . . . ?
 Cl16 B16 B21 Cl21 -0.7(3) . . . . ?
 Cl16 B16 B21 B15 108.8(2) . . . . ?
 Cl16 B16 B21 B17 -112.7(2) . . . . ?
 Cl16 B16 B21 B20 146.3(2) . . . . ?
 Cl16 B16 B21 B22 -149.9(2) . . . . ?
 Cl17 B17 B18 Cl18 -2.9(3) . . . . ?
 Cl17 B17 B18 B12 -111.1(2) . . . . ?
 Cl17 B17 B18 B13 -148.9(2) . . . . ?
 Cl17 B17 B18 B19 147.83(19) . . . . ?
 Cl17 B17 B18 B22 111.2(2) . . . . ?
 Cl17 B17 B21 Cl21 -0.5(3) . . . . ?
 Cl17 B17 B21 B15 148.07(19) . . . . ?
 Cl17 B17 B21 B16 110.2(2) . . . . ?
 Cl17 B17 B21 B20 -148.23(19) . . . . ?
 Cl17 B17 B21 B22 -111.5(2) . . . . ?
 Cl17 B17 B22 Cl22 0.5(3) . . . . ?
 Cl17 B17 B22 B18 -111.7(2) . . . . ?
 Cl17 B17 B22 B19 -148.76(19) . . . . ?
 Cl17 B17 B22 B20 147.23(19) . . . . ?
 Cl17 B17 B22 B21 110.5(2) . . . . ?
 Cl18 B18 B19 Cl19 2.8(3) . . . . ?
 Cl18 B18 B19 B13 -107.7(2) . . . . ?
 Cl18 B18 B19 B14 -145.48(19) . . . . ?
 Cl18 B18 B19 B20 151.90(19) . . . . ?
 Cl18 B18 B19 B22 114.5(2) . . . . ?
 Cl18 B18 B22 Cl22 2.1(3) . . . . ?
 Cl18 B18 B22 B17 111.3(2) . . . . ?
 Cl18 B18 B22 B19 -109.9(2) . . . . ?
 Cl18 B18 B22 B20 -147.4(2) . . . . ?
 Cl18 B18 B22 B21 149.0(2) . . . . ?
 Cl19 B19 B20 Cl20 0.9(3) . . . . ?
 Cl19 B19 B20 B14 -110.7(2) . . . . ?
 Cl19 B19 B20 B15 -148.06(19) . . . . ?
 Cl19 B19 B20 B21 149.14(19) . . . . ?
 Cl19 B19 B20 B22 111.9(2) . . . . ?
 Cl19 B19 B22 Cl22 -0.3(3) . . . . ?
 Cl19 B19 B22 B17 148.1(2) . . . . ?
 Cl19 B19 B22 B18 111.1(2) . . . . ?
 Cl19 B19 B22 B20 -110.6(2) . . . . ?
 Cl19 B19 B22 B21 -148.2(2) . . . . ?
 Cl20 B20 B21 Cl21 -0.7(3) . . . . ?
 Cl20 B20 B21 B15 -110.2(2) . . . . ?
 Cl20 B20 B21 B16 -148.34(19) . . . . ?
 Cl20 B20 B21 B17 147.86(19) . . . . ?
 Cl20 B20 B21 B22 111.3(2) . . . . ?
 Cl20 B20 B22 Cl22 -1.1(3) . . . . ?
 Cl20 B20 B22 B17 -147.44(19) . . . . ?
 Cl20 B20 B22 B18 148.75(19) . . . . ?
 Cl20 B20 B22 B19 111.3(2) . . . . ?
 Cl20 B20 B22 B21 -110.7(2) . . . . ?
 Cl21 B21 B22 Cl22 -1.9(3) . . . . ?
 Cl21 B21 B22 B17 -111.7(2) . . . . ?
 Cl21 B21 B22 B18 -149.54(19) . . . . ?
 Cl21 B21 B22 B19 146.79(19) . . . . ?
 Cl21 B21 B22 B20 109.1(2) . . . . ?
 C16 B12 B13 Cl13 111.1(2) . . . . ?
 C16 B12 B13 B14 -33.05(18) . . . . ?
 C16 B12 B13 B18 -134.0(2) . . . . ?
 C16 B12 B13 B19 -96.2(2) . . . . ?
 C16 B12 B16 Cl16 -111.6(2) . . . . ?
 C16 B12 B16 B15 32.66(18) . . . . ?
 C16 B12 B16 B17 133.8(2) . . . . ?
 C16 B12 B16 B21 95.8(2) . . . . ?
 C16 B12 B17 Cl17 -149.83(19) . . . . ?
 C16 B12 B17 B16 -39.45(18) . . . . ?
 C16 B12 B17 B18 98.8(2) . . . . ?
 C16 B12 B17 B21 -2.2(2) . . . . ?
 C16 B12 B17 B22 61.1(2) . . . . ?
 C16 B12 B18 Cl18 148.27(18) . . . . ?
 C16 B12 B18 B13 39.40(18) . . . . ?
 C16 B12 B18 B17 -98.6(2) . . . . ?
 C16 B12 B18 B19 1.9(2) . . . . ?
 C16 B12 B18 B22 -61.1(2) . . . . ?
 C16 B13 B14 Cl14 110.6(2) . . . . ?
 C16 B13 B14 B15 -32.40(18) . . . . ?
 C16 B13 B14 B19 -134.0(2) . . . . ?
 C16 B13 B14 B20 -96.3(2) . . . . ?
 C16 B13 B18 Cl18 -149.22(19) . . . . ?
 C16 B13 B18 B12 -39.28(18) . . . . ?
 C16 B13 B18 B17 -1.7(3) . . . . ?
 C16 B13 B18 B19 98.7(2) . . . . ?
 C16 B13 B18 B22 61.3(2) . . . . ?
 C16 B13 B19 Cl19 150.39(19) . . . . ?
 C16 B13 B19 B14 39.31(17) . . . . ?
 C16 B13 B19 B18 -98.4(2) . . . . ?
 C16 B13 B19 B20 2.7(2) . . . . ?
 C16 B13 B19 B22 -60.8(2) . . . . ?
 C16 B14 B15 Cl15 111.0(2) . . . . ?
 C16 B14 B15 B16 -33.11(18) . . . . ?
 C16 B14 B15 B20 -134.0(2) . . . . ?
 C16 B14 B15 B21 -95.5(2) . . . . ?
 C16 B14 B19 Cl19 -150.43(19) . . . . ?
 C16 B14 B19 B13 -39.57(17) . . . . ?
 C16 B14 B19 B18 -2.0(2) . . . . ?
 C16 B14 B19 B20 99.1(2) . . . . ?
 C16 B14 B19 B22 61.3(2) . . . . ?
 C16 B14 B20 Cl20 149.90(19) . . . . ?
 C16 B14 B20 B15 39.53(18) . . . . ?
 C16 B14 B20 B19 -98.9(2) . . . . ?
 C16 B14 B20 B21 1.6(2) . . . . ?
 C16 B14 B20 B22 -61.3(2) . . . . ?
 C16 B15 B16 Cl16 110.6(2) . . . . ?
 C16 B15 B16 B12 -32.76(18) . . . . ?
 C16 B15 B16 B17 -96.2(2) . . . . ?
 C16 B15 B16 B21 -133.6(2) . . . . ?
 C16 B15 B20 Cl20 -151.39(18) . . . . ?
 C16 B15 B20 B14 -39.24(18) . . . . ?
 C16 B15 B20 B19 -2.1(2) . . . . ?
 C16 B15 B20 B21 97.8(2) . . . . ?
 C16 B15 B20 B22 60.8(2) . . . . ?
 C16 B15 B21 Cl21 151.41(18) . . . . ?
 C16 B15 B21 B16 39.32(17) . . . . ?
 C16 B15 B21 B17 1.9(2) . . . . ?
 C16 B15 B21 B20 -98.9(2) . . . . ?
 C16 B15 B21 B22 -61.6(2) . . . . ?
 C16 B16 B17 Cl17 151.36(18) . . . . ?
 C16 B16 B17 B12 39.60(18) . . . . ?
 C16 B16 B17 B18 2.5(3) . . . . ?
 C16 B16 B17 B21 -98.2(2) . . . . ?
 C16 B16 B17 B22 -60.9(2) . . . . ?
 C16 B16 B21 Cl21 -149.04(19) . . . . ?
 C16 B16 B21 B15 -39.55(17) . . . . ?
 C16 B16 B21 B17 99.0(2) . . . . ?
 C16 B16 B21 B20 -2.0(3) . . . . ?
 C16 B16 B21 B22 61.8(2) . . . . ?
 B12 C16 B13 Cl13 -108.5(2) . . . . ?
 B12 C16 B13 B14 142.4(2) . . . . ?
 B12 C16 B13 B18 39.78(19) . . . . ?
 B12 C16 B13 B19 102.5(2) . . . . ?
 B12 C16 B14 Cl14 -143.71(19) . . . . ?
 B12 C16 B14 B13 -36.63(19) . . . . ?
 B12 C16 B14 B15 107.0(2) . . . . ?
 B12 C16 B14 B19 3.5(3) . . . . ?
 B12 C16 B14 B20 66.8(2) . . . . ?
 B12 C16 B15 Cl15 144.62(19) . . . . ?
 B12 C16 B15 B14 -106.0(2) . . . . ?
 B12 C16 B15 B16 36.2(2) . . . . ?
 B12 C16 B15 B20 -66.2(2) . . . . ?
 B12 C16 B15 B21 -3.6(3) . . . . ?
 B12 C16 B16 Cl16 107.2(2) . . . . ?
 B12 C16 B16 B15 -143.0(2) . . . . ?
 B12 C16 B16 B17 -40.15(18) . . . . ?
 B12 C16 B16 B21 -102.9(2) . . . . ?
 B12 B13 B14 Cl14 143.68(19) . . . . ?
 B12 B13 B14 C16 33.07(18) . . . . ?
 B12 B13 B14 B15 0.7(3) . . . . ?
 B12 B13 B14 B19 -100.9(2) . . . . ?
 B12 B13 B14 B20 -63.3(2) . . . . ?
 B12 B13 B18 Cl18 -109.9(2) . . . . ?
 B12 B13 B18 B17 37.53(19) . . . . ?
 B12 B13 B18 B19 138.0(2) . . . . ?
 B12 B13 B18 B22 100.6(2) . . . . ?
 B12 B13 B19 Cl19 -148.5(2) . . . . ?
 B12 B13 B19 B14 100.4(2) . . . . ?
 B12 B13 B19 B18 -37.33(18) . . . . ?
 B12 B13 B19 B20 63.8(2) . . . . ?
 B12 B13 B19 B22 0.3(3) . . . . ?
 B12 B16 B17 Cl17 111.8(2) . . . . ?
 B12 B16 B17 B18 -37.06(19) . . . . ?
 B12 B16 B17 B21 -137.7(2) . . . . ?
 B12 B16 B17 B22 -100.5(2) . . . . ?
 B12 B16 B21 Cl21 149.67(19) . . . . ?
 B12 B16 B21 B15 -100.8(2) . . . . ?
 B12 B16 B21 B17 37.74(18) . . . . ?
 B12 B16 B21 B20 -63.3(2) . . . . ?
 B12 B16 B21 B22 0.5(3) . . . . ?
 B12 B17 B18 Cl18 108.1(2) . . . . ?
 B12 B17 B18 B13 -37.86(19) . . . . ?
 B12 B17 B18 B19 -101.1(2) . . . . ?
 B12 B17 B18 B22 -137.8(2) . . . . ?
 B12 B17 B21 Cl21 -148.46(19) . . . . ?
 B12 B17 B21 B15 0.1(3) . . . . ?
 B12 B17 B21 B16 -37.70(19) . . . . ?
 B12 B17 B21 B20 63.8(2) . . . . ?
 B12 B17 B21 B22 100.6(2) . . . . ?
 B12 B17 B22 Cl22 149.58(19) . . . . ?
 B12 B17 B22 B18 37.41(19) . . . . ?
 B12 B17 B22 B19 0.3(3) . . . . ?
 B12 B17 B22 B20 -63.7(2) . . . . ?
 B12 B17 B22 B21 -100.4(2) . . . . ?
 B12 B18 B19 Cl19 148.36(19) . . . . ?
 B12 B18 B19 B13 37.85(19) . . . . ?
 B12 B18 B19 B14 0.1(3) . . . . ?
 B12 B18 B19 B20 -62.5(2) . . . . ?
 B12 B18 B19 B22 -99.9(2) . . . . ?
 B12 B18 B22 Cl22 -146.7(2) . . . . ?
 B12 B18 B22 B17 -37.52(19) . . . . ?
 B12 B18 B22 B19 101.3(2) . . . . ?
 B12 B18 B22 B20 63.8(2) . . . . ?
 B12 B18 B22 B21 0.3(3) . . . . ?
 B13 C16 B12 Cl12 108.7(2) . . . . ?
 B13 C16 B12 B16 -143.0(2) . . . . ?
 B13 C16 B12 B17 -102.9(2) . . . . ?
 B13 C16 B12 B18 -40.01(18) . . . . ?
 B13 C16 B14 Cl14 -107.1(2) . . . . ?
 B13 C16 B14 B15 143.6(2) . . . . ?
 B13 C16 B14 B19 40.13(18) . . . . ?
 B13 C16 B14 B20 103.4(2) . . . . ?
 B13 C16 B15 Cl15 -145.02(19) . . . . ?
 B13 C16 B15 B14 -35.6(2) . . . . ?
 B13 C16 B15 B16 106.6(2) . . . . ?
 B13 C16 B15 B20 4.1(3) . . . . ?
 B13 C16 B15 B21 66.8(2) . . . . ?
 B13 C16 B16 Cl16 143.4(2) . . . . ?
 B13 C16 B16 B12 36.2(2) . . . . ?
 B13 C16 B16 B15 -106.8(2) . . . . ?
 B13 C16 B16 B17 -4.0(3) . . . . ?
 B13 C16 B16 B21 -66.7(2) . . . . ?
 B13 B12 B16 Cl16 -144.29(19) . . . . ?
 B13 B12 B16 C16 -32.72(18) . . . . ?
 B13 B12 B16 B15 -0.1(3) . . . . ?
 B13 B12 B16 B17 101.1(2) . . . . ?
 B13 B12 B16 B21 63.0(2) . . . . ?
 B13 B12 B17 Cl17 148.92(19) . . . . ?
 B13 B12 B17 B16 -100.7(2) . . . . ?
 B13 B12 B17 B18 37.56(19) . . . . ?
 B13 B12 B17 B21 -63.4(2) . . . . ?
 B13 B12 B17 B22 -0.1(3) . . . . ?
 B13 B12 B18 Cl18 108.9(2) . . . . ?
 B13 B12 B18 B17 -138.0(2) . . . . ?
 B13 B12 B18 B19 -37.51(18) . . . . ?
 B13 B12 B18 B22 -100.5(2) . . . . ?
 B13 B14 B15 Cl15 143.39(19) . . . . ?
 B13 B14 B15 C16 32.42(18) . . . . ?
 B13 B14 B15 B16 -0.7(3) . . . . ?
 B13 B14 B15 B20 -101.6(2) . . . . ?
 B13 B14 B15 B21 -63.1(2) . . . . ?
 B13 B14 B19 Cl19 -110.9(2) . . . . ?
 B13 B14 B19 B18 37.52(18) . . . . ?
 B13 B14 B19 B20 138.6(2) . . . . ?
 B13 B14 B19 B22 100.8(2) . . . . ?
 B13 B14 B20 Cl20 -148.43(19) . . . . ?
 B13 B14 B20 B15 101.2(2) . . . . ?
 B13 B14 B20 B19 -37.23(19) . . . . ?
 B13 B14 B20 B21 63.3(2) . . . . ?
 B13 B14 B20 B22 0.3(3) . . . . ?
 B13 B18 B19 Cl19 110.5(2) . . . . ?
 B13 B18 B19 B14 -37.76(18) . . . . ?
 B13 B18 B19 B20 -100.4(2) . . . . ?
 B13 B18 B19 B22 -137.8(2) . . . . ?
 B13 B18 B22 Cl22 149.49(19) . . . . ?
 B13 B18 B22 B17 -101.3(2) . . . . ?
 B13 B18 B22 B19 37.49(19) . . . . ?
 B13 B18 B22 B20 0.0(3) . . . . ?
 B13 B18 B22 B21 -63.6(2) . . . . ?
 B13 B19 B20 Cl20 148.58(19) . . . . ?
 B13 B19 B20 B14 37.02(19) . . . . ?
 B13 B19 B20 B15 -0.4(3) . . . . ?
 B13 B19 B20 B21 -63.2(2) . . . . ?
 B13 B19 B20 B22 -100.5(2) . . . . ?
 B13 B19 B22 Cl22 -148.8(2) . . . . ?
 B13 B19 B22 B17 -0.4(3) . . . . ?
 B13 B19 B22 B18 -37.47(19) . . . . ?
 B13 B19 B22 B20 100.8(2) . . . . ?
 B13 B19 B22 B21 63.3(2) . . . . ?
 B14 C16 B12 Cl12 145.22(19) . . . . ?
 B14 C16 B12 B13 36.57(19) . . . . ?
 B14 C16 B12 B16 -106.4(2) . . . . ?
 B14 C16 B12 B17 -66.3(2) . . . . ?
 B14 C16 B12 B18 -3.4(3) . . . . ?
 B14 C16 B13 Cl13 109.0(2) . . . . ?
 B14 C16 B13 B12 -142.4(2) . . . . ?
 B14 C16 B13 B18 -102.7(2) . . . . ?
 B14 C16 B13 B19 -39.97(18) . . . . ?
 B14 C16 B15 Cl15 -109.4(2) . . . . ?
 B14 C16 B15 B16 142.2(2) . . . . ?
 B14 C16 B15 B20 39.73(18) . . . . ?
 B14 C16 B15 B21 102.4(2) . . . . ?
 B14 C16 B16 Cl16 -146.67(19) . . . . ?
 B14 C16 B16 B12 106.2(2) . . . . ?
 B14 C16 B16 B15 -36.9(2) . . . . ?
 B14 C16 B16 B17 66.0(2) . . . . ?
 B14 C16 B16 B21 3.2(3) . . . . ?
 B14 B13 B18 Cl18 149.76(19) . . . . ?
 B14 B13 B18 B12 -100.3(2) . . . . ?
 B14 B13 B18 B17 -62.8(3) . . . . ?
 B14 B13 B18 B19 37.70(18) . . . . ?
 B14 B13 B18 B22 0.3(3) . . . . ?
 B14 B13 B19 Cl19 111.1(2) . . . . ?
 B14 B13 B19 B18 -137.7(2) . . . . ?
 B14 B13 B19 B20 -36.61(19) . . . . ?
 B14 B13 B19 B22 -100.1(2) . . . . ?
 B14 B15 B16 Cl16 143.77(19) . . . . ?
 B14 B15 B16 C16 33.22(18) . . . . ?
 B14 B15 B16 B12 0.5(3) . . . . ?
 B14 B15 B16 B17 -63.0(2) . . . . ?
 B14 B15 B16 B21 -100.4(2) . . . . ?
 B14 B15 B20 Cl20 -112.1(2) . . . . ?
 B14 B15 B20 B19 37.15(19) . . . . ?
 B14 B15 B20 B21 137.0(2) . . . . ?
 B14 B15 B20 B22 100.1(2) . . . . ?
 B14 B15 B21 Cl21 -147.75(19) . . . . ?
 B14 B15 B21 B16 100.2(2) . . . . ?
 B14 B15 B21 B17 62.8(2) . . . . ?
 B14 B15 B21 B20 -38.01(18) . . . . ?
 B14 B15 B21 B22 -0.8(3) . . . . ?
 B14 B19 B20 Cl20 111.6(2) . . . . ?
 B14 B19 B20 B15 -37.40(19) . . . . ?
 B14 B19 B20 B21 -100.2(2) . . . . ?
 B14 B19 B20 B22 -137.5(2) . . . . ?
 B14 B19 B22 Cl22 147.8(2) . . . . ?
 B14 B19 B22 B17 -63.8(2) . . . . ?
 B14 B19 B22 B18 -100.9(2) . . . . ?
 B14 B19 B22 B20 37.43(19) . . . . ?
 B14 B19 B22 B21 -0.1(3) . . . . ?
 B14 B20 B21 Cl21 147.90(19) . . . . ?
 B14 B20 B21 B15 38.36(18) . . . . ?
 B14 B20 B21 B16 0.3(3) . . . . ?
 B14 B20 B21 B17 -63.5(2) . . . . ?
 B14 B20 B21 B22 -100.1(2) . . . . ?
 B14 B20 B22 Cl22 -150.02(19) . . . . ?
 B14 B20 B22 B17 63.6(2) . . . . ?
 B14 B20 B22 B18 -0.2(3) . . . . ?
 B14 B20 B22 B19 -37.67(18) . . . . ?
 B14 B20 B22 B21 100.4(2) . . . . ?
 B15 C16 B12 Cl12 -144.77(19) . . . . ?
 B15 C16 B12 B13 106.6(2) . . . . ?
 B15 C16 B12 B16 -36.4(2) . . . . ?
 B15 C16 B12 B17 3.7(3) . . . . ?
 B15 C16 B12 B18 66.6(2) . . . . ?
 B15 C16 B13 Cl13 144.6(2) . . . . ?
 B15 C16 B13 B12 -106.8(2) . . . . ?
 B15 C16 B13 B14 35.6(2) . . . . ?
 B15 C16 B13 B18 -67.1(3) . . . . ?
 B15 C16 B13 B19 -4.4(3) . . . . ?
 B15 C16 B14 Cl14 109.3(2) . . . . ?
 B15 C16 B14 B13 -143.6(2) . . . . ?
 B15 C16 B14 B19 -103.5(2) . . . . ?
 B15 C16 B14 B20 -40.18(18) . . . . ?
 B15 C16 B16 Cl16 -109.8(2) . . . . ?
 B15 C16 B16 B12 143.0(2) . . . . ?
 B15 C16 B16 B17 102.9(2) . . . . ?
 B15 C16 B16 B21 40.10(18) . . . . ?
 B15 B14 B19 Cl19 147.97(19) . . . . ?
 B15 B14 B19 B13 -101.2(2) . . . . ?
 B15 B14 B19 B18 -63.6(2) . . . . ?
 B15 B14 B19 B20 37.48(19) . . . . ?
 B15 B14 B19 B22 -0.3(3) . . . . ?
 B15 B14 B20 Cl20 110.4(2) . . . . ?
 B15 B14 B20 B19 -138.4(2) . . . . ?
 B15 B14 B20 B21 -37.95(18) . . . . ?
 B15 B14 B20 B22 -100.9(2) . . . . ?
 B15 B16 B17 Cl17 -147.46(19) . . . . ?
 B15 B16 B17 B12 100.8(2) . . . . ?
 B15 B16 B17 B18 63.7(2) . . . . ?
 B15 B16 B17 B21 -36.97(18) . . . . ?
 B15 B16 B17 B22 0.2(2) . . . . ?
 B15 B16 B21 Cl21 -109.5(2) . . . . ?
 B15 B16 B21 B17 138.6(2) . . . . ?
 B15 B16 B21 B20 37.56(19) . . . . ?
 B15 B16 B21 B22 101.4(2) . . . . ?
 B15 B20 B21 Cl21 109.5(2) . . . . ?
 B15 B20 B21 B16 -38.10(19) . . . . ?
 B15 B20 B21 B17 -101.9(2) . . . . ?
 B15 B20 B21 B22 -138.5(2) . . . . ?
 B15 B20 B22 Cl22 146.40(19) . . . . ?
 B15 B20 B22 B17 0.1(2) . . . . ?
 B15 B20 B22 B18 -63.8(2) . . . . ?
 B15 B20 B22 B19 -101.2(2) . . . . ?
 B15 B20 B22 B21 36.78(18) . . . . ?
 B15 B21 B22 Cl22 -148.17(19) . . . . ?
 B15 B21 B22 B17 102.0(2) . . . . ?
 B15 B21 B22 B18 64.2(2) . . . . ?
 B15 B21 B22 B19 0.5(3) . . . . ?
 B15 B21 B22 B20 -37.14(18) . . . . ?
 B16 C16 B12 Cl12 -108.3(2) . . . . ?
 B16 C16 B12 B13 143.0(2) . . . . ?
 B16 C16 B12 B17 40.13(18) . . . . ?
 B16 C16 B12 B18 103.0(2) . . . . ?
 B16 C16 B13 Cl13 -144.7(2) . . . . ?
 B16 C16 B13 B12 -36.1(2) . . . . ?
 B16 C16 B13 B14 106.3(2) . . . . ?
 B16 C16 B13 B18 3.6(3) . . . . ?
 B16 C16 B13 B19 66.3(2) . . . . ?
 B16 C16 B14 Cl14 146.41(19) . . . . ?
 B16 C16 B14 B13 -106.5(2) . . . . ?
 B16 C16 B14 B15 37.1(2) . . . . ?
 B16 C16 B14 B19 -66.4(2) . . . . ?
 B16 C16 B14 B20 -3.1(3) . . . . ?
 B16 C16 B15 Cl15 108.4(2) . . . . ?
 B16 C16 B15 B14 -142.2(2) . . . . ?
 B16 C16 B15 B20 -102.5(2) . . . . ?
 B16 C16 B15 B21 -39.82(18) . . . . ?
 B16 B12 B13 Cl13 143.82(19) . . . . ?
 B16 B12 B13 C16 32.68(18) . . . . ?
 B16 B12 B13 B14 -0.4(3) . . . . ?
 B16 B12 B13 B18 -101.3(2) . . . . ?
 B16 B12 B13 B19 -63.5(2) . . . . ?
 B16 B12 B17 Cl17 -110.4(2) . . . . ?
 B16 B12 B17 B18 138.3(2) . . . . ?
 B16 B12 B17 B21 37.29(18) . . . . ?
 B16 B12 B17 B22 100.6(2) . . . . ?
 B16 B12 B18 Cl18 -150.52(19) . . . . ?
 B16 B12 B18 B13 100.6(2) . . . . ?
 B16 B12 B18 B17 -37.39(19) . . . . ?
 B16 B12 B18 B19 63.1(2) . . . . ?
 B16 B12 B18 B22 0.1(3) . . . . ?
 B16 B15 B20 Cl20 147.86(19) . . . . ?
 B16 B15 B20 B14 -100.0(2) . . . . ?
 B16 B15 B20 B19 -62.8(2) . . . . ?
 B16 B15 B20 B21 37.02(18) . . . . ?
 B16 B15 B20 B22 0.1(2) . . . . ?
 B16 B15 B21 Cl21 112.1(2) . . . . ?
 B16 B15 B21 B17 -37.38(18) . . . . ?
 B16 B15 B21 B20 -138.2(2) . . . . ?
 B16 B15 B21 B22 -100.9(2) . . . . ?
 B16 B17 B18 Cl18 145.5(2) . . . . ?
 B16 B17 B18 B12 37.36(19) . . . . ?
 B16 B17 B18 B13 -0.5(3) . . . . ?
 B16 B17 B18 B19 -63.7(2) . . . . ?
 B16 B17 B18 B22 -100.4(2) . . . . ?
 B16 B17 B21 Cl21 -110.8(2) . . . . ?
 B16 B17 B21 B15 37.84(19) . . . . ?
 B16 B17 B21 B20 101.5(2) . . . . ?
 B16 B17 B21 B22 138.3(2) . . . . ?
 B16 B17 B22 Cl22 -146.93(19) . . . . ?
 B16 B17 B22 B18 100.9(2) . . . . ?
 B16 B17 B22 B19 63.8(2) . . . . ?
 B16 B17 B22 B20 -0.2(2) . . . . ?
 B16 B17 B22 B21 -36.87(18) . . . . ?
 B16 B21 B22 Cl22 147.13(19) . . . . ?
 B16 B21 B22 B17 37.32(18) . . . . ?
 B16 B21 B22 B18 -0.5(3) . . . . ?
 B16 B21 B22 B19 -64.1(2) . . . . ?
 B16 B21 B22 B20 -101.8(2) . . . . ?
 B17 B12 B13 Cl13 -152.76(19) . . . . ?
 B17 B12 B13 C16 96.1(2) . . . . ?
 B17 B12 B13 B14 63.0(2) . . . . ?
 B17 B12 B13 B18 -37.90(19) . . . . ?
 B17 B12 B13 B19 -0.1(3) . . . . ?
 B17 B12 B16 Cl16 114.6(2) . . . . ?
 B17 B12 B16 C16 -133.8(2) . . . . ?
 B17 B12 B16 B15 -101.2(2) . . . . ?
 B17 B12 B16 B21 -38.07(19) . . . . ?
 B17 B12 B18 Cl18 -113.1(2) . . . . ?
 B17 B12 B18 B13 138.0(2) . . . . ?
 B17 B12 B18 B19 100.5(2) . . . . ?
 B17 B12 B18 B22 37.46(18) . . . . ?
 B17 B16 B21 Cl21 111.9(2) . . . . ?
 B17 B16 B21 B15 -138.6(2) . . . . ?
 B17 B16 B21 B20 -101.0(2) . . . . ?
 B17 B16 B21 B22 -37.22(18) . . . . ?
 B17 B18 B19 Cl19 -148.36(19) . . . . ?
 B17 B18 B19 B13 101.1(2) . . . . ?
 B17 B18 B19 B14 63.4(2) . . . . ?
 B17 B18 B19 B20 0.7(3) . . . . ?
 B17 B18 B19 B22 -36.65(19) . . . . ?
 B17 B18 B22 Cl22 -109.2(2) . . . . ?
 B17 B18 B22 B19 138.8(2) . . . . ?
 B17 B18 B22 B20 101.3(2) . . . . ?
 B17 B18 B22 B21 37.77(19) . . . . ?
 B17 B21 B22 Cl22 109.8(2) . . . . ?
 B17 B21 B22 B18 -37.80(19) . . . . ?
 B17 B21 B22 B19 -101.5(2) . . . . ?
 B17 B21 B22 B20 -139.2(2) . . . . ?
 B18 B12 B13 Cl13 -114.9(2) . . . . ?
 B18 B12 B13 C16 134.0(2) . . . . ?
 B18 B12 B13 B14 100.9(2) . . . . ?
 B18 B12 B13 B19 37.77(19) . . . . ?
 B18 B12 B16 Cl16 152.31(19) . . . . ?
 B18 B12 B16 C16 -96.1(2) . . . . ?
 B18 B12 B16 B15 -63.5(2) . . . . ?
 B18 B12 B16 B17 37.71(19) . . . . ?
 B18 B12 B16 B21 -0.4(3) . . . . ?
 B18 B12 B17 Cl17 111.4(2) . . . . ?
 B18 B12 B17 B16 -138.3(2) . . . . ?
 B18 B12 B17 B21 -101.0(2) . . . . ?
 B18 B12 B17 B22 -37.69(19) . . . . ?
 B18 B13 B14 Cl14 -153.43(18) . . . . ?
 B18 B13 B14 C16 96.0(2) . . . . ?
 B18 B13 B14 B15 63.6(2) . . . . ?
 B18 B13 B14 B19 -38.02(19) . . . . ?
 B18 B13 B14 B20 -0.4(3) . . . . ?
 B18 B13 B19 Cl19 -111.2(2) . . . . ?
 B18 B13 B19 B14 137.7(2) . . . . ?
 B18 B13 B19 B20 101.1(2) . . . . ?
 B18 B13 B19 B22 37.67(19) . . . . ?
 B18 B17 B21 Cl21 148.75(19) . . . . ?
 B18 B17 B21 B15 -62.7(2) . . . . ?
 B18 B17 B21 B16 -100.5(2) . . . . ?
 B18 B17 B21 B20 1.0(3) . . . . ?
 B18 B17 B21 B22 37.80(18) . . . . ?
 B18 B17 B22 Cl22 112.2(2) . . . . ?
 B18 B17 B22 B19 -37.06(19) . . . . ?
 B18 B17 B22 B20 -101.1(2) . . . . ?
 B18 B17 B22 B21 -137.8(2) . . . . ?
 B18 B19 B20 Cl20 -148.35(19) . . . . ?
 B18 B19 B20 B14 100.1(2) . . . . ?
 B18 B19 B20 B15 62.7(2) . . . . ?
 B18 B19 B20 B21 -0.1(3) . . . . ?
 B18 B19 B20 B22 -37.39(19) . . . . ?
 B18 B19 B22 Cl22 -111.4(2) . . . . ?
 B18 B19 B22 B17 37.04(19) . . . . ?
 B18 B19 B22 B20 138.3(2) . . . . ?
 B18 B19 B22 B21 100.7(2) . . . . ?
 B19 B13 B14 Cl14 -115.4(2) . . . . ?
 B19 B13 B14 C16 134.0(2) . . . . ?
 B19 B13 B14 B15 101.6(2) . . . . ?
 B19 B13 B14 B20 37.64(19) . . . . ?
 B19 B13 B18 Cl18 112.1(2) . . . . ?
 B19 B13 B18 B12 -138.0(2) . . . . ?
 B19 B13 B18 B17 -100.5(2) . . . . ?
 B19 B13 B18 B22 -37.44(19) . . . . ?
 B19 B14 B15 Cl15 -152.84(19) . . . . ?
 B19 B14 B15 C16 96.2(2) . . . . ?
 B19 B14 B15 B16 63.1(2) . . . . ?
 B19 B14 B15 B20 -37.84(19) . . . . ?
 B19 B14 B15 B21 0.7(3) . . . . ?
 B19 B14 B20 Cl20 -111.2(2) . . . . ?
 B19 B14 B20 B15 138.4(2) . . . . ?
 B19 B14 B20 B21 100.5(2) . . . . ?
 B19 B14 B20 B22 37.57(19) . . . . ?
 B19 B18 B22 Cl22 112.0(2) . . . . ?
 B19 B18 B22 B17 -138.8(2) . . . . ?
 B19 B18 B22 B20 -37.54(19) . . . . ?
 B19 B18 B22 B21 -101.1(2) . . . . ?
 B19 B20 B21 Cl21 -149.15(19) . . . . ?
 B19 B20 B21 B15 101.3(2) . . . . ?
 B19 B20 B21 B16 63.2(2) . . . . ?
 B19 B20 B21 B17 -0.6(3) . . . . ?
 B19 B20 B21 B22 -37.18(18) . . . . ?
 B19 B20 B22 Cl22 -112.4(2) . . . . ?
 B19 B20 B22 B17 101.3(2) . . . . ?
 B19 B20 B22 B18 37.49(19) . . . . ?
 B19 B20 B22 B21 138.0(2) . . . . ?
 B20 B14 B15 Cl15 -115.0(2) . . . . ?
 B20 B14 B15 C16 134.0(2) . . . . ?
 B20 B14 B15 B16 100.9(2) . . . . ?
 B20 B14 B15 B21 38.52(19) . . . . ?
 B20 B14 B19 Cl19 110.5(2) . . . . ?
 B20 B14 B19 B13 -138.6(2) . . . . ?
 B20 B14 B19 B18 -101.1(2) . . . . ?
 B20 B14 B19 B22 -37.82(19) . . . . ?
 B20 B15 B16 Cl16 -153.48(18) . . . . ?
 B20 B15 B16 C16 96.0(2) . . . . ?
 B20 B15 B16 B12 63.2(2) . . . . ?
 B20 B15 B16 B17 -0.2(2) . . . . ?
 B20 B15 B16 B21 -37.62(18) . . . . ?
 B20 B15 B21 Cl21 -109.7(2) . . . . ?
 B20 B15 B21 B16 138.2(2) . . . . ?
 B20 B15 B21 B17 100.8(2) . . . . ?
 B20 B15 B21 B22 37.26(19) . . . . ?
 B20 B19 B22 Cl22 110.4(2) . . . . ?
 B20 B19 B22 B17 -101.2(2) . . . . ?
 B20 B19 B22 B18 -138.3(2) . . . . ?
 B20 B19 B22 B21 -37.56(19) . . . . ?
 B20 B21 B22 Cl22 -111.0(2) . . . . ?
 B20 B21 B22 B17 139.2(2) . . . . ?
 B20 B21 B22 B18 101.4(2) . . . . ?
 B20 B21 B22 B19 37.69(19) . . . . ?
 B21 B15 B16 Cl16 -115.9(2) . . . . ?
 B21 B15 B16 C16 133.6(2) . . . . ?
 B21 B15 B16 B12 100.8(2) . . . . ?
 B21 B15 B16 B17 37.41(18) . . . . ?
 B21 B15 B20 Cl20 110.8(2) . . . . ?
 B21 B15 B20 B14 -137.0(2) . . . . ?
 B21 B15 B20 B19 -99.9(2) . . . . ?
 B21 B15 B20 B22 -36.93(18) . . . . ?
 B21 B16 B17 Cl17 -110.5(2) . . . . ?
 B21 B16 B17 B12 137.7(2) . . . . ?
 B21 B16 B17 B18 100.7(2) . . . . ?
 B21 B16 B17 B22 37.22(18) . . . . ?
 B21 B17 B18 Cl18 -151.9(2) . . . . ?
 B21 B17 B18 B12 100.0(2) . . . . ?
 B21 B17 B18 B13 62.1(3) . . . . ?
 B21 B17 B18 B19 -1.1(3) . . . . ?
 B21 B17 B18 B22 -37.76(19) . . . . ?
 B21 B17 B22 Cl22 -110.1(2) . . . . ?
 B21 B17 B22 B18 137.8(2) . . . . ?
 B21 B17 B22 B19 100.7(2) . . . . ?
 B21 B17 B22 B20 36.69(18) . . . . ?
 B21 B20 B22 Cl22 109.6(2) . . . . ?
 B21 B20 B22 B17 -36.72(18) . . . . ?
 B21 B20 B22 B18 -100.5(2) . . . . ?
 B21 B20 B22 B19 -138.0(2) . . . . ?
 B22 B17 B18 Cl18 -114.1(2) . . . . ?
 B22 B17 B18 B12 137.8(2) . . . . ?
 B22 B17 B18 B13 99.9(2) . . . . ?
 B22 B17 B18 B19 36.66(19) . . . . ?
 B22 B17 B21 Cl21 111.0(2) . . . . ?
 B22 B17 B21 B15 -100.5(2) . . . . ?
 B22 B17 B21 B16 -138.3(2) . . . . ?
 B22 B17 B21 B20 -36.75(18) . . . . ?
 B22 B18 B19 Cl19 -111.7(2) . . . . ?
 B22 B18 B19 B13 137.8(2) . . . . ?
 B22 B18 B19 B14 100.0(2) . . . . ?
 B22 B18 B19 B20 37.40(19) . . . . ?
 B22 B19 B20 Cl20 -111.0(2) . . . . ?
 B22 B19 B20 B14 137.5(2) . . . . ?
 B22 B19 B20 B15 100.1(2) . . . . ?
 B22 B19 B20 B21 37.29(18) . . . . ?
 B22 B20 B21 Cl21 -112.0(2) . . . . ?
 B22 B20 B21 B15 138.5(2) . . . . ?
 B22 B20 B21 B16 100.4(2) . . . . ?
 B22 B20 B21 B17 36.60(18) . . . . ?
 C17 C18 C19 C20 0.2(5) . . . . ?
 C18 C17 C22 C21 1.0(4) . . . . ?
 C18 C17 C22 C23 -176.4(3) . . . . ?
 C18 C19 C20 C21 -0.1(5) . . . . ?
 C19 C20 C21 C22 0.5(5) . . . . ?
 C20 C21 C22 C17 -0.9(5) . . . . ?
 C20 C21 C22 C23 176.4(3) . . . . ?
 C22 C17 C18 C19 -0.7(5) . . . . ?
 C24 C25 C26 C27 -1.4(6) . . . . ?
 C25 C24 C29 C28 0.7(6) . . . . ?
 C25 C24 C29 C30 175.3(5) . . . . ?
 C25 C26 C27 C28 2.9(7) . . . . ?
 C26 C27 C28 C29 -2.6(8) . . . . ?
 C27 C28 C29 C24 0.9(7) . . . . ?
 C27 C28 C29 C30 -174.1(5) . . . . ?
 C29 C24 C25 C26 -0.4(5) . . . . ?
 C24A C25A C26A C27A -1.5(12) . . . . ?
 C25A C24A C29A C28A -0.3(19) . . . . ?
 C25A C24A C29A C30A 174.0(10) . . . . ?
 C25A C26A C27A C28A 7(2) . . . . ?
 C26A C27A C28A C29A -10(3) . . . . ?
 C27A C28A C29A C24A 6(3) . . . . ?
 C27A C28A C29A C30A -166.1(19) . . . . ?
 C29A C24A C25A C26A -2.1(10) . . . . ?

_olex2_submission_special_instructions  'No special instructions were received'
