data_xcif


  
_exptl_absorpt_correction_type    multi-scan 
_exptl_absorpt_process_details    'SADABS, Sheldrick (2003)' 
_computing_data_collection        'SMART, Bruker (2002)'
_computing_cell_refinement        'SHELXTL, Sheldrick (2001)' 
_computing_data_reduction         'SHELXTL, Sheldrick (2001)'
_computing_structure_solution     'SHELXTL, Sheldrick (2001)' 
_computing_structure_refinement   'SHELXTL, Sheldrick (2001)'
_computing_molecular_graphics     'SHELXTL, Sheldrick (2001)'
_computing_publication_material   'SHELXTL, Sheldrick (2001)'

  
_exptl_special_details 
; 
Data collection is performed with four batch runs at 
φ = 0.00 ° (600 frames), at φ = 90.00 °
(600 frames), at φ = 180 ° (600 frames) and
at φ = 270 ° (600 frames).
Frame width = 0.30 \& in ω. Data is 
merged, corrected for decay, and treated with 
multi-scan absorption corrections. 
; 
  
_diffrn_standards_number          ? 
_diffrn_standards_decay_%         <1 
_diffrn_radiation_probe          X-ray
_diffrn_measurement_device_type  'Bruker AXS APEX diffractometer'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean 836.6
